首页> 外国专利> ULTRAPURE POLYCARBONATES HAVING GOOD NATURAL COLOUR AND HIGH THERMAL STABILITY, APPARATUS AND METHOD FOR PRODUCTION THEREOF

ULTRAPURE POLYCARBONATES HAVING GOOD NATURAL COLOUR AND HIGH THERMAL STABILITY, APPARATUS AND METHOD FOR PRODUCTION THEREOF

机译:具有良好的自然色和高热稳定性的超纯碳酸盐,装置及其生产方法

摘要

FIELD: chemistry.;SUBSTANCE: invention relates to an apparatus for separating an aromatic polycarbonate from a solution obtained via interphase synthesis, which comprises an extruder with a vent for released gases with at least three degassing zones and a carrier agent dispersion zone, wherein the apparatus further includes a descending tubular evaporator and a foam evaporator and said extruder and evaporators are arranged in the series: descending tubular evaporator - foam evaporator - extruder with a vent for released gases, and the carrier agent dispersion zone is located before each degassing zone. Also described is a method of separating an aromatic polycarbonate from a solution obtained via interphase synthesis.;EFFECT: polycarbonates separated using said method, having extremely low residual content of volatile components and thermal decomposition products, as well as improved optical properties, particularly an optimum yellowness index and high thermal stability.;7 cl, 4 dwg, 6 ex
机译:用于从通过相间合成获得的溶液中分离芳族聚碳酸酯的设备技术领域本发明涉及一种用于从通过相间合成获得的溶液中分离芳族聚碳酸酯的设备,该设备包括具有排气口的挤出机,该排气口具有用于释放气体的排气口,该排气口具有至少三个脱气区和载体剂分散区,其中该装置进一步包括下降管式蒸发器和泡沫蒸发器,并且所述挤出机和蒸发器按以下顺序布置:下降管式蒸发器-泡沫蒸发器-具有用于释放气体的排气口的挤出机,并且载体剂分散区位于每个脱气区之前。还描述了从通过相间合成获得的溶液中分离芳族聚碳酸酯的方法。效果:使用所述方法分离的聚碳酸酯具有极低的挥发性组分和热分解产物的残留含量,以及改善的光学性质,特别是最优的黄度指数和高热稳定性。; 7 cl,4 dwg,6 ex

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