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Manufacturing method of water-based environmental resistant coating using sintering aid

机译:利用烧结助剂的水性环保涂料的制造方法

摘要

A method for making an environmental barrier coating (12) using a sintering aid comprising: applying a bond coat layer (14) to a ceramic component (10); combining at least water, and a primary transition material comprising a rare earth disilicate, or a doped rare earth disilicate to produce a transition layer slurry; combining at least water, and a primary outer material comprising a rare earth monosilicate or a doped rare earth monosilicate to produce an outer layer slurry; combining at least water, and a primary compliant material comprising BSAS or a rare earth doped BSAS to produce a compliant layer slurry; applying at least the transition layer slurry, and any one or more of the outer layer slurry or the compliant layer slurry, to the component (10); drying the component; infiltrating a sol-gel solution comprising an aqueous solution of a water soluble salt sintering aid, or an organic solvent solution of a solvent soluble salt sintering aid into the applied slurry layers; and sintering the component to produce the environmental barrier coating (12) having at least the bond coat layer (14), a transition layer (16) and any one or more of an outer layer (20) or a compliant layer (18) wherein during sintering a reaction between the primary materials and the sintering aid results in the transition layer comprising a porosity of from 0% to about 15% by volume of the transition layer, the outer layer comprising a porosity of from 0% to about 30% by volume of the outer layer, and the compliant layer comprising a porosity of from about 0% to about 30% by volume of the compliant layer.
机译:一种使用烧结助剂的环保涂层(12)的方法,包括:将粘结涂层(14)施加到陶瓷部件(10)上;至少将水与包含稀土二硅酸盐或掺杂稀土二硅酸盐的初级过渡材料混合以产生过渡层浆料;结合至少水和包含稀土单硅酸盐或掺杂稀土单硅酸盐的主要外部材料以产生外层浆料;至少将水与包含BSAS或稀土掺杂的BSAS的主要顺应性材料混合,以产生顺应性层浆料;将至少过渡层浆料和外层浆料或柔顺层浆料中的任何一种或多种施加到组分(10)上;干燥组分;将包含水溶性盐烧结助剂的水溶液或溶剂可溶性盐烧结助剂的有机溶剂溶液的溶胶-凝胶溶液渗透到所施加的浆料层中;烧结该部件以产生至少具有粘结涂层(14),过渡层(16)以及外层(20)或柔顺层(18)中的任何一个或多个的环境屏障涂层(12),其中在烧结期间,主要材料和烧结助剂之间的反应导致过渡层的孔隙率为过渡层体积的0%至约15%,外层的孔隙率为0%至约30%(按体积计)外层的体积比为约0%至约30%(体积)。

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