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Method for producing ferromagnetic particle powder, anisotropic magnet, bonded magnet, and dust magnet

机译:铁磁性粒子粉末,各向异性磁体,粘结磁体和粉尘磁体的制造方法

摘要

The present invention relates to ferromagnetic particles capable of exhibiting a high purity and excellent magnetic properties from the industrial viewpoints and a process for producing the ferromagnetic particles, and also provides an anisotropic magnet, a bonded magnet and a compacted magnet which are obtained by using the ferromagnetic particles. The ferromagnetic particles comprising an Fe 16 N 2 compound phase in an amount of not less than 80% as measured by Mössbauer spectrum and each having an outer shell in which FeO is present in the form of a layer having a thickness of not more than 5 nm according to the present invention can be produced by subjecting aggregated particles of an iron compound as a starting material whose primary particles have a ratio of [(average deviation of major axis lengths of particles)/(average major axis length of particles)] of not more than 50%, U c of not more than 1.55, C g of not less than 0.95, C g 2 of not less than 0.40, an average major axis length of 40 to 5000 nm, and an aspect ratio (major axis diameter/minor axis diameter) of 1 to 200, to dispersing treatment; then subjecting the iron compound particles passed through a mesh screen to reducing treatment at a temperature of 160 to 420°C; and subjecting the resulting particles to nitridation treatment at a temperature of 130 to 170°C.
机译:从工业的角度来看,本发明涉及能够显示高纯度和优异的磁性能的铁磁颗粒及其制备方法,并且还提供了通过使用该方法获得的各向异性磁体,粘结磁体和压实磁体。铁磁颗粒。铁磁性颗粒,其具有通过莫斯堡尔光谱测量的不少于80%的Fe 16 N 2化合物相,并且每个均具有外壳,其中FeO以厚度不大于5的层的形式存在。通过使铁化合物的凝集颗粒作为起始材料,其原始颗粒的比率为[(颗粒的长轴长度的平均偏差)/(颗粒的长轴平均长度)],可以制造本发明的nm。不大于50%,U c不大于1.55,C g不小于0.95,C g 2不小于0.40,平均长轴长度为40至5000nm,并且长宽比(长轴直径) /最小轴直径)为1至200,以进行分散处理;然后使通过筛网的铁化合物颗粒在160至420℃的温度下进行还原处理。将得到的颗粒在130至170℃的温度下进行氮化处理。

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