首页> 外国专利> PROCESS FOR SYNTHESISING NANOPARTICLES OF MESOPOROUS AND HOLLOW MAGNETITE OF HIGH SUPERFICIAL AREA IN A SINGLE STEP BY THE AEROSOL ASSISTED CHEMICAL VAPOUR DEPOSITION TECHNIQUE.

PROCESS FOR SYNTHESISING NANOPARTICLES OF MESOPOROUS AND HOLLOW MAGNETITE OF HIGH SUPERFICIAL AREA IN A SINGLE STEP BY THE AEROSOL ASSISTED CHEMICAL VAPOUR DEPOSITION TECHNIQUE.

机译:气溶胶辅助化学气相沉积技术一步法合成高表面积微孔和空心磁铁矿的过程。

摘要

The present invention refers to the obtention of magnetite manoparticles having a hollow and mesoporous structure, which were obtained by the aerosol assisted chemical vapour deposition process, using a precursor solution containing an organic or inorganic salt that contains Fe and a suitable solvent. The synthesis is performed at a temperature of from about 200°C and 900°C, using a mixture of inert and oxidant gases as dragging gas. The nanoparticles obtained by this method are collected and washed with methanol in an ultrasonic bath for being subsequently used.
机译:本发明涉及使用具有有机或无机盐的前体溶液获得具有空心和中孔结构的磁铁矿微粒,所述微粒通过气雾辅助化学气相沉积法获得,所述前体溶液包含含有Fe的有机或无机盐和合适的溶剂。使用惰性气体和氧化剂气体的混合物作为牵引气体,在约200℃至900℃的温度下进行合成。收集通过该方法获得的纳米颗粒,并在超声浴中用甲醇洗涤,以随后使用。

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