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METHOD FOR PREPARING NITROGEN-DOPED GRAPHENE AND NITROGEN-DOPED GRAPHENE PREPARED THEREBY

机译:掺氮石墨烯的制备方法及由此制备的掺氮石墨烯

摘要

The present invention relates to a method for preparing nitrogen-doped graphene, the method comprising: a first step for preparing a mixed solution containing carbon atoms and nitrogen atoms by putting a carbon compound and an amine compound into an acidic solution, followed by heating, stirring, and thermal decomposition; a second step for forming a compound containing carbon atoms, nitrogen atoms, and Fe2+, and then obtaining the compound, the compound being formed by adding an Fe2+-containing solution to the mixed solution containing carbon atoms and nitrogen atoms, followed by stirring; a third step for forming an Fe substrate by thermally treating the compound, which is obtained in the second step, under a nitrogen ambience; and a fourth step for forming nitrogen-doped graphene by, after the third step, diffusing the carbon atoms and the nitrogen atoms, which are contained in the compound, into the Fe substrate through cooling. More preferably, the method further comprises a fifth step for removing, after the fourth step, the Fe substrate by adding an acid to cause a reaction.
机译:本发明涉及一种制备氮掺杂石墨烯的方法,该方法包括:第一步,通过将碳化合物和胺化合物放入酸性溶液中,然后加热,制备包含碳原子和氮原子的混合溶液。搅拌和热分解;第二步是形成含有碳原子,氮原子和Fe 2 + 的化合物,然后得到该化合物,该化合物是通过添加Fe 2 + -而形成的将该溶液加入到含有碳原子和氮原子的混合溶液中,然后搅拌;第三步骤,通过在氮气气氛下热处理在第二步骤中获得的化合物来形成Fe衬底。第四步骤是在第三步骤之后,通过冷却将化合物中所含的碳原子和氮原子扩散到Fe基体中来形成氮掺杂石墨烯。更优选地,该方法进一步包括第五步骤,在第四步骤之后,通过添加酸以引起反应来去除Fe底物。

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