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METHOD FOR PRODUCING DIALKYL POLYSULFIDE, DIALKYL POLYSULFIDE, EXTREME-PRESSURE ADDITIVE AND LUBRICATING FLUID COMPOSITION
METHOD FOR PRODUCING DIALKYL POLYSULFIDE, DIALKYL POLYSULFIDE, EXTREME-PRESSURE ADDITIVE AND LUBRICATING FLUID COMPOSITION
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机译:制备二烷基聚硫化物,二烷基聚硫化物,极压添加剂和润滑流体组合物的方法
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摘要
For the purpose of efficiently producing a dialkyl polysulfide which is able to be favorably used as an extreme-pressure additive which does not easily corrode the metal surface, and an extreme-pressure additive and lubricating fluid composition including the dialkyl polysulfide, provided is a method for producing dialkyl polysulfide including a first step of reacting an olefin compound (a) represented by General Formula (1): R 1 R 2 C=CHR 3 (where R 1 and R 2 each are an alkyl group, R 3 is a hydrogen atom or an alkyl group, and the total number of carbon atoms of R 1 , R 2 and R 3 is 2 to 20) with sulfur in the presence of a hydrogen sulfide to thereby obtain crude dialkyl polysulfide (A), and a second step of reacting the crude dialkyl polysulfide (A) and a sulfide of an alkali metal in a solvent including an alcohol to thereby reduce the number of sulfur atoms in the crude dialkyl polysulfide (A).
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机译:为了有效地生产能够有利地用作不易腐蚀金属表面的极压添加剂的二烷基多硫化物,以及提供一种包括该二烷基多硫化物的极压添加剂和润滑液组合物的方法用于制备多烷基二硫化物的方法,包括使通式(1)表示的烯烃化合物(a)反应的第一步:R 1 R 2 C = CHR 3(其中R 1和R 2各自为烷基,R 3为氢原子或烷基,并且R 1,R 2和R 3的碳原子总数为2至20),在硫化氢存在下用硫磺制得粗制的二烷基多硫化物(A),然后进行第二步使粗二烷基多硫化物(A)与碱金属的硫化物在包含醇的溶剂中反应从而减少粗二烷基多硫化物(A)中的硫原子数的方法。
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