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Precursor of iron catalyst for synthesis of ammonia, with the structure of wustite and method for obtaining of the precursor of iron catalyst with the structure of wustite, for synthesis of ammonia

机译:具有针铁矿结构的用于合成氨的铁催化剂的前体和用于合成氨的具有针铁矿结构的铁催化剂的前体的获得方法

摘要

catalyst precursor containing ferric chloride, in the form of phase wustytowu0105 and oxides promoters is characterized by the fact that contains cobalt oxide (ii) in quantities of from 2 to 5 weight%. the precursor contains oxides promoters in quantities of al2o3 from 2,2% by weight. to 4,5% w / w, cao from 1.7 wt%. to 2.8% by weight. and k2o from 0.4 wt%. to 0.9 wt%.process to obtain a catalyst precursor ferro cobalt on structure of wustytu ammonia synthesis of iron oxides in the presence of a reducing agent to the drowning, promoters, chilling and fragmenting the cast, characterised by the fact that during melting, the cobalt oxide (ii ) in quantities of from 2 to 5 weight%.a pressure regulator is used waste ferric catalyst ammonia synthesis in a quantity of from 15 to 30% relative to iron oxides. as promoters used al2o3 in quantities from 2,2% to 4.5% by weight, cao in quantities from 1.7% to 2.8% by weight and kno3 in quantities of from 0.4% to 0.9% by weight.
机译:以相形式为wustytow10和氧化物促进剂的含氯化铁的催化剂前体的特征在于,其含有2至5重量%的氧化钴(ii)。所述前体包含的氧化物助催化剂的含量为2.2重量%的氧化铝。到4.5%w / w,cao从1.7 wt%。至2.8%(重量)。和k2o为0.4重量%。到0.9重量%的方法,以在还原剂的存在下,在淹没,促进剂,冷却和破碎铸件的还原剂的存在下,在氧化铁的乌斯蒂图氨合成结构上获得催化剂前体铁钴,其特征在于在熔融过程中,氧化钴(ii)的量为2至5重量%。压力调节剂用于废铁催化剂氨的合成,相对于氧化铁为15至30%。作为促进剂,al2o3的用量为2.2%至4.5%重量,cao的用量为1.7%至2.8%重量,kno3的用量为0.4%至0.9%重量。

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