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Process controlled a material surface solid filler and additives to produce a material filler product treated surface chemical reaction

机译:过程控制物料表面的固体填料和添加剂,以产生物料填料产品处理过的表面化学反应

摘要

A process for preparing a material filler product surface treated with succinic anhydride (s), the process comprising comprising at least the steps of: a) Providing at least one filler containing calcium carbonate having i) a value of the average particle size in d50 weight in the range from 0.1 .mu.m to 7 .mu.m 5, ii) a top cut (d98) of = 15 microns, iii) a specific surface area (BET) from 0, 5 to 150 m2 / g measured by the method BET nitrogen, and iv) a total content of residual humidity from 0.01 wt% to 1 wt%, based on the total dry weight of at least one filler containing calcium carbonate, b) providing at least one monosubstituted succinic anhydride and optionally at least monosubstituted succinic acid in an amount from 0.1 to 3% by weight, based on the total dry weight of the at least one material load containing calcium carbonate of step a) C) contacting the surface of at least one filler containing calcium carbonate of step a) under mixing, in one or more steps, with the at least one monosubstituted succinic anhydride and at least one acid succinic optionally monosubstituted step b) such a treatment layer comprising at least one monosubstituted succinic anhydride is formed and at least one succinic acid optionally monosubstituted and / or product (s) salt reaction (s ) thereof on the surface of said at least one filler containing calcium carbonate of step a), wherein the temperature before and / or during the step of contacting c) is adjusted so that the temperature is at least 2 ° C above the melting point of at least monosubstituted succinic anhydride and at least one optional monosubstituted succinic acid.
机译:一种制备经琥珀酸酐表面处理的材料填料产品的方法,该方法包括至少以下步骤:a)提供至少一种含碳酸钙的填料,该填料具有i)d50重量的平均粒度值在0.1μm至7μm的范围内5,ii)顶部切角(d98)≤15微米,iii)比表面积(BET)为0、5至150 m2 / g通过BET氮法,和iv)基于至少一种含碳酸钙的填料的总干重,从0.01wt%至1wt%的残留湿度的总含量,b)提供至少一种单取代的琥珀酸酐和任选的至少0.1至3重量%的单取代的琥珀酸,基于至少一种步骤a)C)的包含碳酸钙的物料负载的总干重,其接触至少一种包含碳酸钙的填料的表面步骤a)在一个或多个步骤中与至少一种单取代的琥珀酸酐和至少一种酸式琥珀酸任选地单取代的步骤b),形成包含至少一种单取代琥珀酸酐的处理层,并且至少一种任选地单取代的琥珀酸和/或其产物的盐反应在步骤a)的所述至少一种含碳酸钙的填料的表面上,调节接触步骤c)之前和/或过程中的温度,使得温度至少比熔点高出至少2℃。单取代的琥珀酸酐和至少一种任选的单取代的琥珀酸。

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