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METHOD FOR DETECTING CONTENT OF FORMALDEHYDE IN TOFU SKIN

机译:检测豆腐皮中甲醛含量的方法

摘要

A method for detecting the content of formaldehyde in tofu skin, comprising the following steps: weighing 10 g of a tofu skin sample, adding a small amount of a stabilizer, shaking evenly and standing in an environment of 30-38 degrees for 50 mins; adding 10-15 ml of deionized water, placing in an ultrasonic cleaning machine for ultrasonic extraction, retrieving a filtrate; then placing same in an ultrasonic oscillator for 20 mins; fetching 5 ml of the filtrate into a flask, then adding ferric ammonium sulfate powder, shaking slightly the flask until all of the powder is dissolved; placing in water of 100 degrees away from light and heating for 35-50 mins; retrieving the reacted sample liquid, and standing for 15-25 mins then filtering via a microporous membrane. The product of the sample, when dried and digested by an ultrasonic water bath machine, obviates the need for an organic solvent for extraction, thus reducing loss in a derivative product, reducing labor intensity, saving medicaments, and, with time being reduced, experimental results detected per the method satisfy analysis requirements for the sample, and achieving the goal of quick detection.
机译:一种检测豆腐皮中甲醛含量的方法,包括以下步骤:称量10g豆腐皮样品,加入少量稳定剂,均匀摇动,在30-38度的环境中静置50分钟。加入10-15毫升去离子水,置于超声波清洗机中进行超声波提取,回收滤液。然后将其放在超声波振荡器中20分钟;将5ml滤液倒入烧瓶中,然后加入硫酸铁铵粉末,轻轻摇动烧瓶直至所有粉末溶解。放置在远离光线100度的水中并加热35至50分钟;取出反应的样品液体,静置15-25分钟,然后通过微孔膜过滤。样品的产品经过超声波水浴机干燥和消化后,就不再需要用于萃取的有机溶剂,从而减少了衍生产品的损失,降低了劳动强度,节省了药物,并且随着时间的推移减少了实验性该方法检测到的结果满足样品分析要求,达到了快速检测的目的。

著录项

  • 公开/公告号WO2017114441A1

    专利类型

  • 公开/公告日2017-07-06

    原文格式PDF

  • 申请/专利权人 TIAN LINLIN;

    申请/专利号WO2016CN112832

  • 发明设计人 TIAN LINLIN;

    申请日2016-12-29

  • 分类号G01N30/02;

  • 国家 WO

  • 入库时间 2022-08-21 13:30:31

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