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METHOD FOR PREPARING HIGH-PURITY INDIUM OXIDE FROM INDIUM SCRAPS

机译:从铟渣中制备高纯度氧化铟的方法

摘要

The present invention relates to a method for preparing high-purity indium oxide from indium scraps. The method according to the present invention comprises the steps of: pulverizing indium scraps into a predetermined size to obtain powder of indium scraps; an indium scrap-dissolving and residue-removing step in which an inorganic acid is introduced to the pulverized powdery indium scraps to dissolve the indium scraps and removing the insoluble residue; a precipitating agent-introducing and metal hydroxide-precipitating step in which a precipitating agent is introduced to the acid solution from which the insoluble residue is removed to precipitate a metal hydroxide with a pH of 3-9; an organic acid-introducing and crystallizing step in which an organic acid is introduced to the metal hydroxide so that it may be crystallized into a metal oxalate; and an indium oxide-forming step in which the crystallized metal oxalate is oxidized in the air. According to the present invention, low-quality indium scraps are pulverized into a predetermined size to produce colloidal particles, which, in turn, are crystallized and oxidized in the air. In this manner, it is possible to high-purity indium oxide. The method according to the present invention generates no waste acid, has a simple working process, and allows eco-friendly and cost-efficient recycle of indium scraps.;COPYRIGHT KIPO 2017
机译:由铟屑制备高纯度氧化铟的方法技术领域本发明涉及由铟屑制备高纯度氧化铟的方法。根据本发明的方法包括以下步骤:将铟屑粉碎成预定尺寸以获得铟屑粉末;和铟屑溶解·残渣去除工序,将无机酸导入粉状的粉状铟屑中,使铟屑溶解,除去不溶性残渣。沉淀剂引入和金属氢氧化物沉淀步骤,其中将沉淀剂引入酸溶液中,从其中除去不溶性残留物,以沉淀出pH值为3-9的金属氢氧化物。引入有机酸和结晶的步骤,其中将有机酸引入到金属氢氧化物中以使其结晶成金属草酸盐。氧化铟形成步骤,其中结晶的草酸金属在空气中被氧化。根据本发明,将低质量的铟屑粉碎成预定尺寸以产生胶体颗粒,该胶体颗粒又在空气中结晶并氧化。以这种方式,可以制备高纯度的氧化铟。根据本发明的方法不产生废酸,具有简单的工作过程,并且允许对铟屑进行生态友好和成本有效的回收。; COPYRIGHT KIPO 2017

著录项

  • 公开/公告号KR20170027588A

    专利类型

  • 公开/公告日2017-03-10

    原文格式PDF

  • 申请/专利权人 LSP. CO. LTD.;

    申请/专利号KR20150124408

  • 发明设计人 LEE CHUL JOOKR;GU SOO JINKR;

    申请日2015-09-02

  • 分类号C01G15/00;

  • 国家 KR

  • 入库时间 2022-08-21 13:27:56

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