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Manufacturing method of quaternary ammonium salt and electric double layer capacitor using the quaternary ammonium salt manufactured by the method

机译:季铵盐的制造方法和使用该方法制造的季铵盐的双电层电容器

摘要

The present invention relates to a process for the production of trimethylmethoxymethylammonium chloride, which comprises the steps of adding trimethylamine and chloromethyl methyl ether to a first solvent and reacting them, and producing a white precipitate, trimethylmethoxymethylammonium chloride, A step of selectively separating trimethylmethoxymethylammonium chloride and tetrafluoroboric acid, and a step of reacting the resulting reaction product with a second solvent to obtain a depressurized distillate; Adding methylene chloride and distilled water to the reduced pressure concentrate, extracting the organic layer, collecting the organic layer and distillation under reduced pressure, and adding the resultant of the vacuum distillation to a third solvent to precipitate the precipitate, then selectively separating the precipitate 111N, the quaternary ammonium salt comprises the step of obtaining a BF 41O1 It relates to an electric double layer capacitor using the manufacturing method and thus the quaternary ammonium salts prepared by.
机译:三甲基甲氧基甲基氯化铵的生产方法技术领域本发明涉及三甲基甲氧基甲基氯化铵的生产方法,其包括将三甲胺和氯甲基甲基醚添加到第一溶剂中并使它们反应,并产生白色沉淀的三甲基甲氧基甲基氯化铵,选择性地分离三甲基甲氧基甲基氯化铵和四氟硼酸,以及使所得反应产物与第二溶剂反应以获得减压馏出物的步骤;在减压浓缩液中加入二氯甲烷和蒸馏水,萃取有机层,收集有机层并在减压下蒸馏,然后将真空蒸馏的所得物添加至第三溶剂中以沉淀出沉淀物,然后选择性地分离沉淀物。 Sub> 111 N,季铵盐包括获得BF 4 1 O1 一种涉及使用该制造方法的双电层电容器,并由此制备的季铵盐。

著录项

  • 公开/公告号KR101745861B1

    专利类型

  • 公开/公告日2017-06-12

    原文格式PDF

  • 申请/专利权人 상명대학교산학협력단;

    申请/专利号KR20140148974

  • 发明设计人 김기택;한태희;

    申请日2014-10-30

  • 分类号C01B35/06;C01B35/08;C01C1/28;

  • 国家 KR

  • 入库时间 2022-08-21 13:25:24

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