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PROCESS FOR THE PREPARATION OF A SOL-GEL SOLUTION USED FOR THE PREPARATION OF A BARIUM TITANATE DOPED BY HAFNIUM AND / OR AT LEAST ONE LANTHANIDE ELEMENT
PROCESS FOR THE PREPARATION OF A SOL-GEL SOLUTION USED FOR THE PREPARATION OF A BARIUM TITANATE DOPED BY HAFNIUM AND / OR AT LEAST ONE LANTHANIDE ELEMENT
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机译:用于制备由HA和/或至少一种镧系元素掺杂的钛酸钡的溶胶-凝胶溶液的制备方法
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摘要
The invention relates to a process for preparing a sol-gel solution for use in the preparation of a hafnium-doped barium titanate ceramic and / or at least one lanthanide element comprising the following steps: a) a a contacting step of a first mixture comprising a barium carboxylate and a diol solvent and a second mixture comprising a titanium alkoxide and a hafnium alkoxide and / or an alkoxide of a lanthanide element in a monoalcoholic solvent; b) a step of distilling the mixture resulting from step a), in order to remove at least a portion of the monoalcoholic solvent; c) a step of adding, hot, acetic acid to the distilled mixture of step b).
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