首页> 外国专利> PROCESS FOR THE PREPARATION OF A SOL-GEL SOLUTION USED FOR THE PREPARATION OF A BARIUM TITANATE DOPED BY HAFNIUM AND / OR AT LEAST ONE LANTHANIDE ELEMENT

PROCESS FOR THE PREPARATION OF A SOL-GEL SOLUTION USED FOR THE PREPARATION OF A BARIUM TITANATE DOPED BY HAFNIUM AND / OR AT LEAST ONE LANTHANIDE ELEMENT

机译:用于制备由HA和/或至少一种镧系元素掺杂的钛酸钡的溶胶-凝胶溶液的制备方法

摘要

The invention relates to a process for preparing a sol-gel solution for use in the preparation of a hafnium-doped barium titanate ceramic and / or at least one lanthanide element comprising the following steps: a) a a contacting step of a first mixture comprising a barium carboxylate and a diol solvent and a second mixture comprising a titanium alkoxide and a hafnium alkoxide and / or an alkoxide of a lanthanide element in a monoalcoholic solvent; b) a step of distilling the mixture resulting from step a), in order to remove at least a portion of the monoalcoholic solvent; c) a step of adding, hot, acetic acid to the distilled mixture of step b).
机译:本发明涉及一种用于制备ha掺杂钛酸钡陶瓷和/或至少一种镧系元素的溶胶-凝胶溶液的方法,该方法包括以下步骤:a)第一混合物的接触步骤,所述第一混合物包括:羧酸钡和二醇溶剂,以及在一元醇溶剂中的第二混合物,所述第二混合物包含钛醇盐和醇盐和/或镧系元素的醇盐。 b)蒸馏步骤a)所得混合物的步骤,以除去至少一部分一元醇溶剂; c)向步骤b)的蒸馏混合物中加入热乙酸的步骤。

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