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Method for preparing a sol-gel solution which can be used for preparing a barium titanate ceramic doped with hafnium and/or with at least one lanthanide element
Method for preparing a sol-gel solution which can be used for preparing a barium titanate ceramic doped with hafnium and/or with at least one lanthanide element
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机译:制备可用于制备掺杂有and和/或至少一种镧系元素的钛酸钡陶瓷的溶胶-凝胶溶液的方法
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摘要
The invention relates to a method for preparing a sol-gel solution which can be used to prepare a barium titanate ceramic doped with hafnium and/or with at least one lanthanide element, comprising the following steps:a) a step to place a first mixture comprising a barium carboxylate and a diol solvent in contact with a second mixture comprising a titanium alkoxide and a hafnium alkoxide and/or an alkoxide of a lanthanide element in a monoalcohol solvent;b) a step to distil the mixture resulting from step a) to remove at least part of the monoalcohol solvent;c) a step to add acetic acid, under heat, to the distilled mixture of step b).展开▼