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Method for preparing ultrahigh-purity silicon carbide powder

机译:超高纯度碳化硅粉的制备方法

摘要

The present invention relates to a method for preparing an ultrahigh-purity silicon carbide powder, more particularly to a method for preparing an ultrahigh-purity silicon carbide granular powder by preparing a gel wherein a silicon compound and a carbon compound are uniformly dispersed via a sol-gel process using a liquid state silicon compound and a solid or liquid state carbon compound of varying purities as raw materials, preparing a silicon dioxide-carbon (SiO2—C) composite by pyrolyzing the prepared gel, preparing a silicon carbide-silicon dioxide-carbon (SiC—SiO2—C) composite powder via two-step carbothermal reduction of the prepared silicon dioxide-carbon composite, adding a silicon metal and then conducting carbonization and carbothermal reduction at the same time by heat treating, thereby growing the synthesized silicon carbide particle with an increased yield of the silicon carbide.
机译:本发明涉及一种制备超高纯度碳化硅粉末的方法,更具体地涉及一种通过制备凝胶而制备超高纯度碳化硅颗粒粉末的方法,其中硅溶胶和碳化合物通过溶胶均匀地分散。液态硅化合物和不同纯度的固态或液态碳化合物作为原料的凝胶法,通过热解制备的凝胶来制备二氧化硅-碳(SiO 2 -C)复合材料,通过两步碳热还原制得的二氧化硅-碳复合材料,添加硅金属,然后进行碳化和碳化,从而制备碳化硅-二氧化硅-碳(SiC-SiO 2 -C)复合粉末。通过热处理同时进行碳热还原,从而以增加的碳化硅收率生长合成的碳化硅颗粒。

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