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Production and characterization of boron carbide and silicon carbide reinforced copper-nickel composites by powder metallurgy method

机译:粉末冶金方法的碳化硼和碳化硅加固铜镍复合材料的生产与鉴定

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摘要

In this study, composite samples were produced by reinforcing boron carbide and silicon carbide particles in different rates by weight into copper-nickel powder mixture using powder metallurgy method. The prepared powder mixtures were cold pressed under 600 MPa pressure and pelletized. The pelletized samples were then sintered in an atmosphere-controlled furnace. Scanning electron microscopy to determine the microstructure of the produced samples and x-ray diffraction method analysis to determine the phases forming in the structure of the produced samples were used and microhardness was taken to determine the effect of boron carbide and silicon carbide on hardness. In addition to that, the mechanical properties the transverse rupture strength were investigated using three-point bending tests. The corrosion tests were performed potentiodynamic polarization curves of the samples in 3.5 % sodium chloride solution. The highest hardness value was measured as 162 HV 0.05 in the sample reinforced with 10 % boron carbide. As the amount of silicon carbide increased, the corrosion resistance of the composite increased. Moreover, as the amount of boron carbide increased, the corrosion resistance of the composite decreased. Load-contact depth values were examined, copper-nickel+10 % silicon carbide has the highest peak depth of 48.12.
机译:在该研究中,通过使用粉末冶金方法将碳化硼和碳化硅颗粒加强碳化硼和碳化硅颗粒以不同的速率加入铜镍粉末混合物来制备复合样品。制备的粉末混合物在600MPa压力下冷却并造粒。然后将粒化样品烧结在气氛控制的炉中。扫描电子显微镜以确定所产生的样品和X射线衍射方法分析的微观结构,以确定所产生的样品结构中形成的相位,并考虑碳化硼和碳化硅对硬度的影响。除此之外,使用三点弯曲试验研究了机械性能横断强度。腐蚀试验在3.5%氯化钠溶液中进行样品的电位偏振曲线。在用10%碳化硼加强的样品中测量最高硬度值为162HV 0.05。随着碳化硅的量增加,复合材料的耐腐蚀性增加。此外,随着碳化硼的量增加,复合材料的耐腐蚀性降低。检查负载接触深度值,铜 - 镍+ 10%碳化硅具有最高峰值深度为48.12。

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