首页> 外国专利> DIRECT AND EFFECTIVE THERMAL METHOD FOR SYNTHESIS OF PEROVSKITE MATERIALS OF THE LACOOTYPE IN AIR, FROM LANTHANUM AND COBALT OXIDIC PRECURSORS

DIRECT AND EFFECTIVE THERMAL METHOD FOR SYNTHESIS OF PEROVSKITE MATERIALS OF THE LACOOTYPE IN AIR, FROM LANTHANUM AND COBALT OXIDIC PRECURSORS

机译:直接有效的热法从镧和钴氧化前体合成空气中Lacootype钙钛矿材料

摘要

The invention relates to a method of synthesis of LaCoO-type perovskite materials. According to the invention, the method comprises the thermal synthesis from solid state in air, starting from a predefined molar mixture of lanthanum and cobalt oxide as powder, having a grain size of 2...6 μ m, by controlled heating in air, at a constant rate of 1...3°K/min, to the synthesis temperature of 750...1000°C, for 8...12 h, to result in LaCoOperovskite powder with highly uniform grains as size, shape and composition, representing at least 98.7% of the total mass of the synthesis product.
机译:本发明涉及LaCoO型钙钛矿材料的合成方法。根据本发明,该方法包括从空气中的固态热合成,其是通过预定的镧和氧化钴的粉末的预定摩尔混合物,其具有2 ...6μm的晶粒尺寸,通过在空气中的受控加热来进行的,以1 ... 3°K / min的恒定速率加热至750 ... 1000°C的合成温度,持续8 ... 12 h,得到的LaCoOperovskite粉末的粒度,形状和形状均非常均匀。组成,至少占合成产物总质量的98.7%。

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