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DIRECT THERMAL METHOD FOR SYNTHESIS OF PEROVSKITE MATERIALS OF THE LACOOTYPE

机译:直接热法合成钙钛矿型钙钛矿材料

摘要

The invention relates to a method of synthesis of LaCoO-type perovskite materials. According to the invention, the method comprises the thermal synthesis from solid state in air, starting from a predefined molar mixture of lanthanum and cobalt oxide as powder, having a grain size of 2...6 μ m, by controlled heating in air, at a constant rate of 1...3°K/min, to the synthesis temperature of 750...1000°C, for 8...12 h, to result in LaCoOperovskite powder with highly uniform grains as size, shape and composition, representing at least 98.7% of the total mass of the synthesis product.
机译:本发明涉及LaCoO型钙钛矿材料的合成方法。根据本发明,该方法包括从空气中的固态热合成,其是通过预定的镧和氧化钴的粉末的预定摩尔混合物,其具有2 ...6μm的晶粒尺寸,通过在空气中的受控加热来进行的,以1 ... 3°K / min的恒定速率加热至750 ... 1000°C的合成温度,持续8 ... 12 h,得到的LaCoOperovskite粉末的粒度,形状和形状均非常均匀。组成,至少占合成产物总质量的98.7%。

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