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METHOD FOR REMOVING IMPURITIES FROM MOTHER LIQUOR OF ISOPHTHALIC ACID USING CRYSTALLIZATION

机译:结晶法去除异邻苯二甲酸母液中杂质的方法

摘要

Disclosed is a method for removing impurities from a mother liquor of isophthalic acid using crystallization, which can remove reaction intermediates generated in an oxidation process of isophthalic acid, and multi-aromatic substances to which the reaction intermediates are bound through crystallization of isophthalic acid, and can separate by-product having a difference in melting point from the mother liquor without further post-treatment. Provided is the method for removing the impurities from the mother liquor of isophthalic acid using crystallization, which comprises the following steps: (a) dissolving a solid component in the mother liquor by heating the mother liquor produced after an isophthalic acid synthesis reaction; (b) supplying heated solution to a crystallizer and cooling the solution for crystallization; and (c) separating the mother liquor and the solid component from the crystallizer and supplying the mother liquor to the isophthalic acid synthesis reaction.;COPYRIGHT KIPO 2018
机译:公开了一种使用结晶从间苯二甲酸的母液中除去杂质的方法,该方法可以去除间苯二甲酸的氧化过程中产生的反应中间体,以及通过间苯二甲酸的结晶而结合有该反应中间体的多芳族物质,以及可以将熔点不同的副产物与母液分离,而无需进一步的后处理。本发明提供了一种通过结晶除去间苯二甲酸母液中的杂质的方法,其包括以下步骤:(a)通过加热间苯二甲酸合成反应后生成的母液,将固体成分溶解在母液中。 (b)将加热的溶液供应到结晶器并冷却该溶液以结晶; (c)从结晶器中分离出母液和固体成分,并将母液提供给间苯二甲酸合成反应。COPYRIGHT KIPO 2018

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