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EPOXY NANOCOMPOSITE REINFORCED WITH GRAPHENE OXIDE DECORATED WITH NANODIAMOND NANOCLUSTER AND METHOD FOR MANUFACTURING THEREOF

机译:纳米金刚石纳米簇修饰的氧化石墨烯增强环氧树脂纳米复合材料的制备方法

摘要

The present invention is obtained by mixing and sonicating the synthesized surface-modified graphene oxide and nanodiamond in ethanol to obtain a stable dispersion, reacted at 60 ° C and filtered to prepare a graphene oxide / nanodiamond composites and then epoxy and curing agent To provide an epoxy composite material with enhanced mechanical strength by mixing with More specifically, (1) oxidizing graphite using a strong acid and an oxidizing agent to synthesize graphene oxide; (2) modifying the surface of the prepared graphene oxide; (3) modifying the surface of the nanodiamond; (4) preparing a graphene oxide composite filler to which nanodiamond nanoclusters are introduced by mixing the prepared surface-modified graphene oxide and nanodiamond; (5) a method for producing an epoxy composite material reinforced with graphene oxide introduced with the nanodiamond nanocluster introduced by mixing the graphene oxide composite filler prepared with the nanodiamond nanocluster prepared above and an epoxy and a curing agent. According to the present invention as described above, by using GN as a filler to add to the epoxy resin, to provide an epoxy composite material with improved mechanical properties even with a small amount of GN filler compared to the epoxy composite reinforced with conventional graphene oxide It works.
机译:通过将合成的表面改性的氧化石墨烯和纳米金刚石在乙醇中混合并超声处理以获得稳定的分散体,然后在60℃下反应并过滤以制备氧化石墨烯/纳米金刚石复合材料,然后通过本发明获得本发明。环氧树脂和固化剂通过与环氧树脂混合,提供一种具有增强的机械强度的环氧复合材料。(1)使用强酸和氧化剂氧化石墨以合成氧化石墨烯; (2)修饰所制备的氧化石墨烯的表面; (3)修饰纳米金刚石的表面; (4)通过混合制备的表面改性的氧化石墨烯和纳米金刚石,制备引入了纳米金刚石纳米团簇的氧化石墨烯复合填料; (5)一种制造方法,该方法通过将通过与以上制备的纳米金刚石纳米团簇制备的氧化石墨烯复合填料和环氧树脂和固化剂混合而引入的引入有纳米金刚石纳米团簇的氧化石墨烯增强的环氧复合材料的制备方法。如上所述,根据本发明,通过使用GN作为填料添加到环氧树脂中,与使用常规氧化石墨烯增强的环氧复合材料相比,即使使用少量的GN填料,也能够提供具有改善的机械性能的环氧复合材料。有用。

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