首页> 外国专利> METHOD FOR PRODUCING ZETA-NEGATIVE NANODIAMOND DISPERSION AND ZETA-NEGATIVE NANODIAMOND DISPERSION

METHOD FOR PRODUCING ZETA-NEGATIVE NANODIAMOND DISPERSION AND ZETA-NEGATIVE NANODIAMOND DISPERSION

机译:制备ZETA负纳米金刚石分散体和ZETA负纳米金刚石分散体的方法

摘要

FIELD: nanotechnologies.;SUBSTANCE: invention relates to nanotechnology. Carboxylated nanodiamond powder is suspended in a liquid medium from a group including polar protic or aprotic solvents, bipolar aprotic solvents, ionic liquids or mixtures thereof, for example, in water. Zeta-potential of the resulting suspension is more than -30 mV at pH from 3 to 5. After that, the pH of the suspension is adjusted to at least 7 by adding a Bronsted or Lewis base, preferably ammonium hydroxide, ammonia. Suspension is then treated with ultrasound and ground in a ball mill. Resulting dispersion contains more than 1 wt% of carboxylated nanodiamonds of single-digit nanometer size and has a zeta potential of more than -35 mV, measured at a pH of more than 7. D90 average primary particle size distribution in the resulting dispersion is 2–30 nm.;EFFECT: method for producing a zeta-negative nanodiamond dispersion and a zeta-negative nanodiamond dispersion are disclosed.;23 cl, 7 dwg, 1 tbl
机译:技术领域:纳米技术。发明涉及纳米技术。将羧化的纳米金刚石粉末从例如极性质子或非质子溶剂,双极性非质子溶剂,离子液体或其混合物中悬浮在液体介质中,例如,在水中。在3至5的pH值下,所得悬浮液的Zeta电位大于-30 mV。此后,通过添加布朗斯台德或路易斯碱(优选氢氧化铵)氨水将悬浮液的pH值调节至至少7。然后将悬浮液用超声波处理并在球磨机中进行研磨。所得分散液包含超过1 wt%的一位数纳米大小的羧化纳米金刚石,且在pH大于7时测得的Zeta电位大于-35 mV。所得分散液中D90的平均初级粒径分布为2 –30 nm。; EFFECT:公开了制备zeta阴性纳米金刚石分散体和zeta阴性纳米金刚石分散体的方法。; 23 cl,7 dwg,1 tbl

著录项

  • 公开/公告号RU2681615C2

    专利类型

  • 公开/公告日2019-03-11

    原文格式PDF

  • 申请/专利权人 KARBODEON LTD OJ;

    申请/专利号RU20150145029

  • 发明设计人 MYULLYUMYAKI VESA (FI);SYUREN JESSE (FI);

    申请日2014-04-22

  • 分类号C01B32/15;C01B32/28;B82B3;B82B1;B82Y40;

  • 国家 RU

  • 入库时间 2022-08-21 11:46:21

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