MONITORING DEVICE FOR MONITORING CHEMICAL REACTIONS USING MR MEASUREMENTS IN A FLOW-THROUGH CELL

摘要

A monitoring device is provided for analytical measurement of reaction fluid produced in a reaction vessel in a spectrometer with a monitoring cell. The distribution apparatus includes at least four supply and return lines that open into the distribution apparatus, wherein the distribution apparatus comprises a distribution device for distributing reaction fluid to the supply and return lines. The distribution apparatus comprises a distribution vessel in which the distribution device and an electrically controllable pump device for pumping of the reaction fluid are provided, wherein the distribution device comprises an electrically controllable valve device for distributing the reaction fluid to the lines that open into the distribution vessel. A control and regulating device for electrical control of the pump device and of the valve device is provided, wherein reaction control is prompt, automated, and optimized with respect to process parameters, and wherein temperature control may include the entire flow path.