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ZNO NANOWIRES INTENDED FOR PHOTOCATALYSIS FOR WATER AND/OR AIR PURIFICATION

机译:旨在光催化水和/或空气净化的ZNO纳米线

摘要

The present invention concerns a method of a growth of ZnO nanowires (6b) intended for photocatalysis in water and/or air depollution, comprising the following steps:- (i) cleaning a civil engineering element (1) having a volume (2) which presents external rough surfaces (4a, 4b, 4c, 4d) with asperities (3);- (ii) immerging the civil engineering element (1) at least partially in a seed layer solution (5) which is an alcoholic solution with ions Zn2+, with at least one given rough surface (4a) facing to the seed layer solution (5) for the impregnation of the given rough surface (4a) with asperities (3) by the seed layer solution (5);- (iii) taking the immerged civil engineering element (1), out of the seed layer solution (5), with the seed layer (5a) coating the asperities (3) of the given rough surface (4a), without controlling the coating thickness of the seed layer (5a) on the given coated rough surface (4a);- (iv) drying the given coated rough surface (4a);- (v) annealing the seed layer coating of the given coated rough surface (4a) to obtain ZnO nanocristallites (6a);- (vi) chemical bath deposition for direct growth of ZnO nanowires (6b) from the ZnO nanocristallites (6a) of the given coated rough surface of the civil engineering element.
机译:本发明涉及用于在水和/或空气污染中进行光催化的ZnO纳米线(6b)的生长方法,其包括以下步骤:-(i)清洁具有一定容积(2)的土木工程元件(1),该容积具有使外部粗糙表面(4a,4b,4c,4d)具有凹凸不平(3);-(ii)将土木工程元件(1)至少部分浸入种子层溶液(5)中,该种子层溶液是具有Zn 2 + 离子的酒精溶液,至少具有一个给定的粗糙表面(4a) )面对种子层溶液(5)以通过种子层溶液(5)浸渍具有凹凸的给定粗糙表面(4a)(3);-(iii)将浸没的土木工程元件(1)从种子层溶液(5)中取出,用种子层(5a)涂覆给定粗糙表面(4a)的凹凸(3),而无需控制涂层在给定的涂覆的粗糙表面(4a)上的种子层(5a)的厚度;-(iv)干燥给定的涂层粗糙表面(4a);-(v)将给定的涂覆的粗糙表面(4a)的晶种层涂层退火,以获得ZnO纳米晶体(6a);-(vi)化学浴沉积,用于从土木工程元件的给定涂层粗糙表面的ZnO纳米晶体(6a)中直接生长ZnO纳米线(6b)。

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