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Effect of Thermal and Microwave Treatment on Low Temperature Mechanical Property of Glass Fiber Reinforced Polymer Composite: An Experimental Exploration

机译:热处理和微波处理对玻璃纤维增​​强聚合物复合材料低温力学性能的影响:实验探索

摘要

There has been a tremendous advancement in the science and technology of fiber reinforced polymer composites (FRP) in recent times. The low density, high strength, high stiffness to weight ratio, excellent durability, and design flexibility of fiber reinforced polymers are the primary reasons for their use in many structural components in the aircrafts, automotive, marine, transportation, sports, medical science and more recently the building and construction industries and particularly in areas that are weight and corrosion sensitive. A recent example is the Bridge-in-a-Backpack for 2014 Winter Olympics in Russia, an innovative inflatable composite-concrete arch bridge, which was developed to reduce construction time and costs, increase lifespan, reduce maintenance costs and reduce the carbon footprint of bridge construction1. But the phenomenon of the occurrence of their fracture and failure at low temperatures and under varying loading rates is a quite complex, and is not easily understandable phenomenon, because of the various types of the failure modes involved (e.g. delamination sites, debonding, fiber pullout regions, crack propagation front, striations and bubble bursting in the matrix). Thus a critical study has to be made to understand the overall phenomenon. Recently an active area of investigation related to this work is being explored by Temperature Modulated Differential Scanning Calorimetry (TMDSC) and Fourier Transform Infrared Spectroscopy (FTIR-Imaging), techniques to find out the possible causes for failure of the composite. In the present study, an attempt has been made for fractographic study of the composite material using SEM micrographs of the fractured surfaces of composites under Thermally Conditioned and post curing by Microwave treatment, followed by their exposure in ultralow temperatures, so that the origin of the crack could be analyzed and the factors affecting the locus of initiation of fracture could be determined. This would be followed by FTIR-Imaging and TMDSC to determine the alternation and deviation of Stoichiometry and the Tg values respectively, to have a better idea about the failure phenomenon.
机译:近年来,纤维增强聚合物复合材料(FRP)的科学和技术取得了巨大的进步。纤维增强聚合物的低密度,高强度,高刚度/重量比,出色的耐用性和设计灵活性是它们在飞机,汽车,船舶,运输,体育,医学等领域的许多结构部件中使用的主要原因最近,建筑业,尤其是对重量和腐蚀敏感的领域。最近的一个例子是俄罗斯2014年冬季奥运会的“后背包桥”,这是一种创新的充气式复合混凝土拱桥,其开发目的是减少施工时间和成本,延长使用寿命,降低维护成本并减少碳足迹。桥梁建设1。但是,由于涉及到各种类型的破坏模式(例如分层,脱胶,纤维拔出),因此在低温和不同的加载速率下,它们的破裂和破坏的发生现象是相当复杂的,并且不容易理解。区域,裂纹扩展前沿,条纹和基体中的气泡破裂)。因此,必须进行批判性研究以了解整体现象。最近,温度调制差示扫描量热法(TMDSC)和傅里叶变换红外光谱(FTIR-Imaging)正在探索与这项工作有关的研究领域,这些技术可以找出复合材料失效的可能原因。在本研究中,已经尝试使用复合材料的断裂表面的SEM显微照片进行复合材料的断裂形貌研究,该复合材料在热条件下经过微波处理后固化,然后将其暴露在超低温下,从而使复合材料的起源成为可能。可以分析裂纹并确定影响断裂起始点的因素。然后,通过FTIR成像和TMDSC分别确定化学计量学和Tg值的交替和偏差,以更好地了解故障现象。

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