Synthesis of 1-(O,O-dialkylphosphorylamido)propyl-5-aza-2,8,9-trioxa-1-silatricyclo-[3,3,3,0(1,5)] undecanes

Li ZH; Song XY

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Synthesis of 1-(O,O-dialkylphosphorylamido)propyl-5-aza-2,8,9-trioxa-1-silatricyclo-[3,3,3,0(1,5)] undecanes

机译：1-（O，O-二烷基磷酰胺基）丙基-5-氮杂-2,8,9-三氧杂-1-硅三环-[3,3,3,0（1,5）]十一烷的合成

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摘要

Ten 1-(O,O-dialkyl phoshorylamido)propyl-5-aza-2,8,9-trioxa-1-sil-atricyclo [3,3,3,0(1.5)] undecanes were synthesized by the reaction of dialkoxy phosphoryl chlorides with aminopropyl silatrane and their structures were established by elemental analysis, IR, (HNMR)-H-1, and MS measurement. The suitable reaction. conditions are discussed based on. the related reaction mechanism.

机译：通过二烷氧基反应合成十个1-（O，O-二烷基磷酰胺基）丙基-5-氮杂-2,8,9-三氧杂-1-硅-三环[3,3,3,0（1.5）]十一烷通过元素分析，IR，（HNMR）-H-1和MS测量，确定了具有氨基丙基甲硅烷基的磷酸氯及其结构。合适的反应。条件的讨论依据。相关的反应机理。

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《Phosphorus, Sulfur, and Silicon and the Related Elements》 |2004年第7期|共6页
作者
Li ZH; Song XY;
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中图分类非金属元素及其化合物;
关键词
organosilicon compound; phosphoroamide; silatrane; SILATRANES;

机译：有机硅化合物;磷酰胺;硅橡胶;硅酮;

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1. Synthesis of 1-(O,O-dialkylphosphorylamido)propyl-5-aza-2,8,9-trioxa-1-silatricyclo-[3,3,3,0(1,5)] undecanes [J] . Li ZH, Song XY Phosphorus, Sulfur, and Silicon and the Related Elements . 2004,第7期

机译：1-（O，O-二烷基磷酰胺基）丙基-5-氮杂-2,8,9-三氧杂-1-硅三环-[3,3,3,0（1,5）]十一烷的合成
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4. Synthesis, Photochromism Properties of 1-(1,5-Dimethyl-2-Pyrrolecarbonitrile)-2-2-Methyl-5-(4-Aminomethyl)Phenyl-3-Thienyl Perfluorocyclopentene [C] . Gang LI, Xue LI, Gang LIU, International Conference on Advanced Material Research and Application . 2017

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Synthesis of 1-(O,O-dialkylphosphorylamido)propyl-5-aza-2,8,9-trioxa-1-silatricyclo-[3,3,3,0(1,5)] undecanes

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