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The impact of tower internals on column performance

机译:塔内件对色谱柱性能的影响

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摘要

Fractionation Research Inc. (FRI) is the most modern independent test institute in the world for performing tray, random packing, and structured packing tests under rectification conditions on an industrial scale test column (see Figure 1). In 1998, Raschig Super-Ring No. 2 was tested at FRI for the first time, and FRI high performance tower internals were selected for this test. However, in 2012, Raschig elected to retest Super-Ring No. 2. In this retest, the company used state of the art tower internals. This article shows the impact of tower internals on packing performance, comparing both FRI test results. In addition to the FRI test results, the article provides information about Raschig's large scale liquid distributor test facility. The test facility was built to improve large and small scale distributor designs as a development project and to demonstrate their performance after fabrication for industrial columns. Finally, the article describes an industrial design example for which modern tower internals were applied.
机译:Fractionation Research Inc.(FRI)是世界上最现代的独立测试机构,用于在工业规模的测试柱上,在精馏条件下进行塔盘,无规填充和规整填充测试(见图1)。 1998年,拉希格2号超级环首次在FRI进行了测试,并选择了FRI高性能塔内件进行此项测试。但是,在2012年,拉希格(Raschig)选择对2号超级指环进行重新测试。在这次重新测试中,该公司使用了最先进的塔内件。本文比较了两个FRI测试结果,显示了塔内部构件对填料性能的影响。除了FRI测试结果外,本文还提供了有关Raschig的大型液体分配器测试设备的信息。测试设施的建立是为了改善大型和小型分配器设计,这是一个开发项目,并证明了在制造工业色谱柱后的性能。最后,本文描述了一个工业设计实例,其中应用了现代塔式内部构件。

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