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OPTICAL METHODS FOR NONDESTRUCTIVE EVALUATION OF SUBSURFACE FLAWS IN SILICON NITRIDE CERAMICS

机译:氮化硅陶瓷中表面缺陷的无损评价光学方法

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摘要

It is known that the strength and lifetime of silicon nitrides are strongly affected by subsurface flaws that are either inherent to the material (voids, porosity, etc.) or induced by component processing such as machining damage (e.g., cracks). Because ceramics are translucent, optical methods are effective to detect and characterize these types of subsurface flaws. In this study, three optical methods were developed/utilized for nondestructive evaluation (NDE) of subsurface flaws in silicon nitride ceramics: (1) laser backscatter, (2) optical coherence tomography (OCT) and, (3) confocal microscopy. The laser backscatter is a two-dimensional method while both OCT and confocal are three-dimensional methods. Subsurface flaws of various types, sizes, and depths can be identified and imaged by these NDE methods. In particular, subsurface Hertzian cracks, induced by surface indentations with various loads, were clearly imaged for the first time by the confocal method. This paper describes these methods and presents NDE data and their correlation with surface photomicrography results.
机译:众所周知,氮化硅的强度和寿命受材料固有的表面缺陷(空隙,孔隙等)或由诸如加工损伤(例如裂纹)之类的零件加工引起的表面缺陷的强烈影响。由于陶瓷是半透明的,因此光学方法可以有效地检测和表征这些类型的表面缺陷。在这项研究中,开发/使用了三种光学方法用于氮化硅陶瓷表面缺陷的无损评估(NDE):( 1)激光反向散射,(2)光学相干断层扫描(OCT)和(3)共聚焦显微镜。激光反向散射是二维方法,而OCT和共聚焦都是三维方法。这些NDE方法可以识别和成像各种类型,大小和深度的地下缺陷。特别是,通过共聚焦方法首次清晰地成像了由各种载荷的表面压痕引起的地下赫兹裂纹。本文介绍了这些方法,并介绍了NDE数据及其与表面显微摄影结果的相关性。

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