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Preparation and Characterization of Tubular Ceramic Support for Use in Transesterification Process

机译:用于酯交换反应的管状陶瓷载体的制备和表征

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A tubular ceramic support intended for use in transesterification process was prepared using the polymeric foam replication method. Pieces of foam with pores 120 ppi in size were completely immersed in a 25wt% solid-loading of porcelain slurry. The dried samples were sintered- for 2 hours to temperatures ranging from 1200°C to 1265°C, respectively. It was found that the optimum sintering temperature was 1250°C as the following values were obtained for each characteristic: 1.98 MPa compressive strength, 47.3% porosity, 2.773 gcm~3 density and 0.45mm pore size. XRD results show that the sintered ceramic consists ofmullite and quartz.
机译:使用聚合泡沫复制方法制备了打算用于酯交换过程的管状陶瓷载体。将尺寸为120 ppi的细孔泡沫完全浸入25%固含量的瓷浆中。将干燥的样品烧结2小时至分别在1200℃至1265℃的温度范围内。发现最佳烧结温度为1250℃,因为针对每个特性获得以下值:1.98MPa抗压强度,47.3%孔隙率,2.773gcm〜3密度和0.45mm孔径。 XRD结果表明,该烧结陶瓷由莫来石和石英组成。

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