The One Pot Synthesis Salicylaldehyde Prepared by Reactive Grinding with Derivative Phenol and Paraformaldehyde in Absence Magnesium Methoxide

EBRAHIM BALALI; ABOLGHASEM SHAMELI; HOSEEIN NAEIMI

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The One Pot Synthesis Salicylaldehyde Prepared by Reactive Grinding with Derivative Phenol and Paraformaldehyde in Absence Magnesium Methoxide

机译：甲醇无镁的衍生物苯酚与多聚甲醛反应研磨一锅合成水杨醛。

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摘要

The formylation phenols are mono-formylated using a mixture of paraformaldehyde, Mg(OMe)2, by reactive grinding. In all cases but one, only one regioisomer of the salicylaldehyde is obtained in good to high yield.

机译：使用多聚甲醛Mg（OMe）2的混合物通过反应研磨将甲酰化酚单甲酰化。在除一种情况以外的所有情况下，仅以良好至高收率获得了水杨醛的一种区域异构体。

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《Oriental Journal of Chemistry: An International Research Journal of Pure & Applied Chemistry 》 |2013年第4期| 共4页
作者
EBRAHIM BALALI; ABOLGHASEM SHAMELI; HOSEEIN NAEIMI;
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正文语种 eng
中图分类化学 ;
关键词
Formylation; Phenols; Regioisomer; Salicylaldehyde; One pot synthesis.;

机译：甲酰化;苯酚;区域异构体;水杨醛;一锅合成;

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1. The One Pot Synthesis Salicylaldehyde Prepared by Reactive Grinding with Derivative Phenol and Paraformaldehyde in Absence Magnesium Methoxide [J] . EBRAHIM BALALI, ABOLGHASEM SHAMELI, HOSEEIN NAEIMI Oriental Journal of Chemistry: An International Research Journal of Pure & Applied Chemistry . 2013 ,第4期

机译：甲醇无镁的衍生物苯酚与多聚甲醛反应研磨一锅合成水杨醛。
2. One-Pot Synthesis of Phenol Derivatives by the Novel Intramolecular Alder–Rickert Reaction: Effects of Aryl Substituent at the 3-Position of Cyclohexenone Derivatives on Reactivity [J] . Chemical and Pharmaceutical Bulletin . 2013 ,第7期

机译：新型分子内Alder-Rickert反应一锅法合成苯酚衍生物：环己烯酮衍生物3-位上的芳基取代基对反应性的影响
3. Reactivity And Hydrogen Storage Performances Of Magnesium-nickel-copper Ternary Mixtures Prepared By Reactive Mechanical Grinding [J] . C, Milanese, A, International journal of hydrogen energy . 2008 ,第17期

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4. One-pot 2 ＋ 2 cyclization/nucleophilic addition of o-alkynyl-O-allenyl phenol leading to cyclobutacchromene derivatives [C] . Shohei Ohno, Avena Ramon, Hiromichi Fujioka 日本化学会春季年会講演予稿集 . 2018

机译：一锅2 + 2环化/亲核加入O-炔基-O-苯甲酸苯酚，其导致Cyclobuta C Chrome衍生物
5. New developments toward the synthesis of heterocycles and applications in green chemistry. I. A simple and essentially one-pot synthesis of N-aminated heterocycles using phase transfer catalyst (Aliquat-336). II. Synthesis of pharmaceutically important pyrrole derivatives. III. Applications in green chemistry: Surfactant-mediated environmentally friendly cleavage of aromatic esters and trans-esterification under solvent-free neutral conditions . [D] . Patel, Nitinchandra. 2005

机译：杂环合成的新进展及其在绿色化学中的应用。 I.使用相转移催化剂（Aliquat-336）简单且基本上一锅合成N-胺化的杂环。二。药学上重要的吡咯衍生物的合成。三，在绿色化学中的应用：在无溶剂的中性条件下，表面活性剂介导的环境友好的芳族酯裂解和酯交换反应。
6. A green and efficient protocol for the synthesis of dihydropyrano23-cpyrazole derivatives via a one-pot four component reaction by grinding method [O] . Sethurajan Ambethkar, Vediappen Padmini, Nattamai Bhuvanesh 2015

机译：通过研磨一锅四组分反应合成二氢吡喃并23-c吡唑衍生物的绿色高效方法
7. A green and efficient protocol for the synthesis of dihydropyrano[2,3-c]pyrazole derivatives via a one-pot, four component reaction by grinding method [O] . Sethurajan Ambethkar, Vediappen Padmini, Nattamai Bhuvanesh 2015

机译：通过研磨法通过一锅四组分反应合成二氢吡喃并[2,3-c]吡唑衍生物的绿色有效方案

The One Pot Synthesis Salicylaldehyde Prepared by Reactive Grinding with Derivative Phenol and Paraformaldehyde in Absence Magnesium Methoxide

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