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首页> 外文期刊>Oriental Journal of Chemistry: An International Research Journal of Pure & Applied Chemistry >Synthesis, characterization of some new 1 -phenyl (3-chloro- 4-methoxy, 2-methoxy-5-methyl)- 4(substituted) phenyl benzene-azo acetyl acetone-3,5-di methyl pyrazoles
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Synthesis, characterization of some new 1 -phenyl (3-chloro- 4-methoxy, 2-methoxy-5-methyl)- 4(substituted) phenyl benzene-azo acetyl acetone-3,5-di methyl pyrazoles

机译:某些新型1-苯基(3-氯-4-甲氧基,2-甲氧基-5-甲基)-4(取代)苯基苯-偶氮乙酰丙酮-3,5-二甲基吡唑的合成,表征

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摘要

This review introduces the synthesis of some newly 1 -phenyl (3-chloro-4-methoxy, 2-methoxy-5-methyl)- 4(substituted) phenyl benzeneazo acetyl acetone-3,5-dimethyl pyrazoles (4a-4l, 5a-5l) containing different selected functional groups have been synthesized by condensing (3-chloro-4-methoxy, 2-methoxy-5-methyl) phenyl benzeneazo acetyl acetone hydrazone (1a,2a) with (R')-malon phenyl anilic acid hydrazide (3a-3i.Sj.Sj,3k.3k1-3l) in alcoholic medium, presence of glacial acetic acid as a catalyst. The identity of newly synthesized compounds were confirmed on the basis of their spectral studies viz- IR, physical properties, elemental analysis.
机译:这篇综述介绍了一些新的1-苯基(3-氯-4-甲氧基,2-甲氧基-5-甲基)-4(取代的)苯基苯偶氮基乙酰丙酮-3,5-二甲基吡唑(4a-4l,5a通过缩合(3-氯-4-甲氧基,2-甲氧基-5-甲基)苯基苯偶氮乙酰丙酮(1a,2a)与(R')-丙二醛苯胺酸来合成含有不同选择官能团的-5l)酰肼(3a-3i.Sj.Sj,3k.3k1-3l)在酒精介质中,以冰醋酸作为催化剂存在。根据新化合物的光谱研究,即红外光谱,物理性质和元素分析,确定了它们的身份。

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