N-(tert-Butoxycarbonyl)-N-[4-(dimethylazaiumylidene)-1,4-dihydropyridin-1-ylsulfonyl]azanide:A New Sulfamoylating Agent.Structure and Reactivity toward Amines

Jean-Yves Winum; Loic Toupet; Veronique Barragan; Georges Dewynter; Jean-Louis Montero

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N-(tert-Butoxycarbonyl)-N-[4-(dimethylazaiumylidene)-1,4-dihydropyridin-1-ylsulfonyl]azanide:A New Sulfamoylating Agent.Structure and Reactivity toward Amines

机译：N-（叔丁氧基羰基）-N- [4-（二甲基氮杂亚苄基）-1,4-二氢吡啶-1-基磺酰基]氮杂叠氮酰胺：一种新型氨磺酰化剂。

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摘要

Synthesis,structure,and reactivity toward amines of the new sulfamoylating reagent 2 are described.Compound 2 allowed sulfamoylation of amines under very mild conditios to give sulfamide derivatives in good yields.

机译：描述了新型氨磺酰化试剂2的合成，结构和对胺的反应性。化合物2允许胺在非常温和的条件下进行氨磺酰化，从而以良好的收率得到磺酰胺衍生物。

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《Organic letters》 |2001年第14期|共3页
作者
Jean-Yves Winum; Loic Toupet; Veronique Barragan; Georges Dewynter; Jean-Louis Montero;
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1. N-(tert-Butoxycarbonyl)-N-[4-(dimethylazaiumylidene)-1,4-dihydropyridin-1-ylsulfonyl]azanide:A New Sulfamoylating Agent.Structure and Reactivity toward Amines [J] . Jean-Yves Winum, Loic Toupet, Veronique Barragan, Organic letters . 2001,第14期

机译：N-（叔丁氧基羰基）-N- [4-（二甲基氮杂亚苄基）-1,4-二氢吡啶-1-基磺酰基]氮杂叠氮酰胺：一种新型氨磺酰化剂。
2. Practical One-Pot Synthesis of N-(tert-Butoxycarbonyl)sulfamide from Chlorosulfonyl Isocyanate via N-(tert-Butoxycarbonyl)aminosulfonylpyridinium Salt [J] . Toshiaki Masui, Mikio Kabaki, Hideaki Watanabe, Organic process research & development . 2004,第3期

机译：实用的N-（叔丁氧羰基）氨基磺酰基吡啶鎓盐由氯磺酰基异氰酸酯一锅法合成N-（叔丁氧羰基）磺酰胺
3. Synthesis of unusual amino acids: N-(tert-butoxycarbonyl)-L-vinyl glycine and N-(tert-butoxycarbonyl)-L-homophenylalanine [J] . Chandrasekhar S., Raza A., Takhi M. Tetrahedron, Asymmetry: The International Journal for Repid Publication on all Aspects of Asymmetry in Orgainc, Inorganic, Organometallic, Physical and Bio-Organic Chemistry . 2002,第4期

机译：异常氨基酸的合成：N-（叔丁氧羰基）-L-乙烯基甘氨酸和N-（叔丁氧羰基）-L-高苯丙氨酸
4. Synthesis, characterization and theoretical study of some transition metal complexes with N-(4-(dimethyl amino benzylidene)benzod thiozal-2-amine) [C] . Sahar S. Hassan, Sura K. Ibrahim, Muhanned A. Mahmoud International Conference on Materials Engineering and Science . 2019

机译：用N-（4-（二甲基氨基苄基）苯并D硫代-2-胺的一些过渡金属配合物的合成，表征和理论研究
5. Synthesis of 4-[(2-chloroethanimidamido) methyl --N- (prop-2-yn-1-yl) benzamide, a possible in vivo activity probe of DDAH-like enzymes [D] . Ratz, Patrick. 2015

机译：DDAH样酶的体内活性探针4-[（2-氯乙亚胺嘧啶基）甲基-N-（prop-2-yn-1-yl）苯甲酰胺的合成
6. Polyμ3-(E)-N-(pyridin-4-ylmethylidene)hydroxylaminato-κ3O:N:N′μ2-(E)-N-(pyridin-4-ylmethylidene)hydroxylamine-κ2N:N′(E)-N-(pyridin-4-ylmethylidene-κN)hydroxylaminedisilver(I) nitrate [O] . Shan Gao, Seik Weng Ng 2012

机译：聚μ3-（E）-N-（吡啶-4-基亚甲基）羟氨基-κ3O：N：N′ μ2-（E）-N-（吡啶-4-基亚甲基）羟胺-κ2N：N （E）-N-（吡啶-4-基亚甲基-κN）羟胺分散剂（I）硝酸盐
7. Synthesis of novel Schiff base N-[(E)-1-(1H-indole-3-yl)methylidene]-N-[4-(4-{[(E)-1-(1H-indol-3-yl)methylidene]amino} phenoxy)phenyl] amine [O] . M. Zarei, A. A. Jarrahpour 2004

机译：新型席夫碱N - [（E）-1-（1H-吲哚-3-基）亚甲基] -N- [4-（4 - {[（E）-1-（1H-吲哚-3-基）]的合成亚甲基]氨基}苯氧基）苯基]胺

N-(tert-Butoxycarbonyl)-N-[4-(dimethylazaiumylidene)-1,4-dihydropyridin-1-ylsulfonyl]azanide:A New Sulfamoylating Agent.Structure and Reactivity toward Amines

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