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Preparation of Mn2O3 catalyst with core-shell structure via spray pyrolysis assisted with glucose

机译:葡萄糖辅助喷雾热解制备核壳型Mn2O3催化剂

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摘要

A novel core-shell Mn2O3 catalyst is obtained by facile spray pyrolysis assisted with glucose acting as a structure-directing agent. The detail characterizations include X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), nitrogen adsorption/desorption isotherms, and the thermogravimetric method (TG/DTA). In the probe test of the aqueous degradation of methylene blue (MB), the high catalytic peroxidization activity of core-shell Mn2O3 catalyst, compared to the commercial Mn2O3, is attributed to the high crystallization of alpha-Mn2O3, the large surface area that resulted from the core-shell structure with porous architecture, and the special core-shell structure that acted as a micro-reactor.
机译:通过以葡萄糖为辅助的轻度喷雾热解,得到了新型的核壳型Mn2O3催化剂。详细特征包括X射线衍射(XRD),扫描电子显微镜(SEM),透射电子显微镜(TEM),氮吸附/解吸等温线和热重法(TG / DTA)。在对亚甲蓝(MB)进行水降解的探针测试中,与市售Mn2O3相比,核-壳Mn2O3催化剂的高催化过氧化活性归因于α-Mn2O3的高结晶化,这导致了较大的表面积从具有多孔结构的核-壳结构,到充当微反应器的特殊核-壳结构。

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