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Extraction of essential oil from Cupressus sempervirens: Comparison of global yields, chemical composition and antioxidant activity obtained by hydrodistillation and supercritical extractionh

机译:从四季柏中提取香精油:通过水蒸馏和超临界萃取获得的全球产量,化学成分和抗氧化活性的比较h

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摘要

In this study, supercritical fluid extraction (SFE) with CO2 and hydrodistillation (HD) were compared as methods to isolate the essential oil from Cupressus sempervirens. The odour of the oil obtained by SFE at 90 bar and 40°C was very close to the odour of the leaves of C. sempervirens before the extraction. Compounds extracted by both SFE and HD were identified by GC-FID and GC-MS. Moreover, the difference in the chemical composition obtained by SFE and HD was quite noticeable qualitatively and quantitatively. Phenolic composition and antioxidant activity were also determined. Compared to HD, the SFE method presents some advantages: the extraction was completed after 1 h in SFE, although 4 h is necessary for HD, and the yield was improved by 34%. Finally, it has also been shown that SFE is very selective towards some specific components such as manoyl oxide, trans-totarol and -acoradiene.
机译:在这项研究中,比较了用CO2和加氢蒸馏(HD)进行超临界流体萃取(SFE)作为从长柏(Cupressus sempervirens)分离精油的方法。通过SFE在90 bar和40°C下获得的油的气味非常接近提取前的emp。sempervirens叶片的气味。通过SFE和HD提取的化合物均通过GC-FID和GC-MS进行鉴定。而且,通过SFE和HD获得的化学成分的差异在定性和定量上都非常明显。还测定了酚类成分和抗氧化活性。与HD相比,SFE方法具有一些优点:尽管在HD中需要4 h,但在SFE中1 h即可完成萃取,并且收率提高了34%。最后,还显示出SFE对某些特定组分如氧化锰,反式-甲苯酚和-二十碳二烯非常有选择性。

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