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Synthesis and magnetic properties of Fe_(0.32)Ni_(0.68) alloy nanotubes

机译:Fe_(0.32)Ni_(0.68)合金纳米管的合成及磁性

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摘要

Fe_(0.32)Ni_(0.68) alloy nanotubes have been successfully synthesized by electrochemical deposition using a polycarbonate membrane template. The transmission electron microscope and scanning electron microscope observations reveal that the nanotubes have a conical morphology with two ends stuffed and a hollow structure. The length and diameter of the nanotubes are 7-8 mu m and 200 nm, respectively. The aspect ratio (length to diameter) is as large as 40. Magnetic measurements show that the coercivities of the nanotubes for an applied parallel and perpendicular field are about 21 and 55 Oe, respectively. The hysteresis loops indicate that the nanotubes were more easily magnetized in applied parallel field than in applied perpendicular field. The mechanism of nucleation and growth of these nanotubes is also discussed.
机译:Fe_(0.32)Ni_(0.68)合金纳米管已成功通过电化学沉积使用聚碳酸酯膜模板合成。透射电子显微镜和扫描电子显微镜的观察表明,纳米管具有圆锥形的形态,其两端被填充并且是中空结构。纳米管的长度和直径分别为7-8μm和200nm。长宽比(长度与直径)最大为40。磁性测量表明,纳米管在施加的平行场和垂直场中的矫顽力分别约为21和55 Oe。磁滞回线表明,在施加的平行场中,纳米管在施加的垂直场中更容易磁化。还讨论了这些纳米管的成核和生长机理。

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