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Synthesis and optical properties of multiwalled carbon nanotubes beaded with Cu_2O nanospheres

机译:含Cu_2O纳米球的多壁碳纳米管的合成及光学性质

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A method for synthesizing multiwalled carbon nanotubes (MWNTs) beaded with C112G nanospheres has been developed. In this work Cu(CH_3COO)_2 centre dot H_2O served as the precursor and NaBH_4 as the reducing agent, and the produced CU_2O nanoparticles were deposited on the MWNTs with the help of poly(vinyl pyrrolidone) (PVP). After increasing the ageing time, grapelike Cu_2O nanospheres adhering to the MWNTs gradually came into being. The synthesized products were systematically studied by x-ray powder diffraction, scanning electron microscopy and transmission electron microscopy. UV-vis absorption spectra were used to estimate the band gap energies of the hybrid system. The synthesis process was facile, efficient and not time-consuming. This method may shed light on integrating MWNTs with other oxide nanospheres and/or nanoparticles using a PVP medium, and lead to an exploration of the potential properties of nanocomposite hybrid materials.
机译:已经开发了一种合成带有C112G纳米球的多壁碳纳米管(MWNT)的方法。在这项工作中,Cu(CH_3COO)_2中心点H_2O作为前体,NaBH_4作为还原剂,并且在聚乙烯吡咯烷酮(PVP)的帮助下,将生成的CU_2O纳米颗粒沉积在MWNT上。随着时间的增长,逐渐形成了附着于多壁碳纳米管的葡萄状Cu_2O纳米球。通过X射线粉末衍射,扫描电子显微镜和透射电子显微镜系统地研究了合成产物。紫外可见吸收光谱被用来估计混合系统的带隙能量。合成过程简便,高效且不费时。该方法可以揭示使用PVP介质将MWNT与其他氧化物纳米球和/或纳米颗粒整合的方法,并导致对纳米复合杂化材料潜在性能的探索。

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