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Mechanichal properties and corrosion resistance of duplex stainless steel forgings with large wall thicknesses

机译:大壁厚双相不锈钢锻件的机械性能和耐蚀性

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Duplex stainless steels are widely used in chemical process, oil and gas industry. One of the main applications are disconnect able mooring systems (SWIVEL connections) for offshore Floating Production Storage and Offloading units (FPSO). Due to the increasing demand for energy ever larger cast or forged parts are required in the offshore industry. It is a well known fact that in larger duplex stainless steel forgings precipitation of detrimental phases can take place, such as Sigma phase or nitrides. Impact strength at low temperature and corrosion resistance will be influenced by these precipitations. Therefore mechanical properties and corrosion resistance of ring rolled products with large wall thicknesses are the main objective of this report. Hence, mechanical properties including impact strength were determined as a function of specimen test location depth in a part that failed during acceptance testing. Additionally two test rings with identical wall thickness and different forging ratios were investigated in the same manner. Corrosion resistance tests were performed according to ASTM G48 and in some cases Critical Pitting Temperature (CPT) was established. The microstructure was examined via Optical Microscopy as well as Scanning Electron Microscopy (SEM) and Transmission Electron Microscopy (TEM). A Focused Ion Beam (FIB) device was used to micromachine TEM foils at evident sites in SEM specimens.
机译:双相不锈钢广泛用于化学过程,石油和天然气工业。主要应用之一是可分离的系泊系统(SWIVEL连接),用于海上浮动生产存储和卸载装置(FPSO)。由于对能源的需求不断增加,海上工业需要更大的铸件或锻件。众所周知的事实是,在较大的双相不锈钢锻件中会发生有害相的析出,例如Sigma相或氮化物。这些沉淀会影响低温下的冲击强度和耐腐蚀性。因此,具有较大壁厚的环轧产品的机械性能和耐腐蚀性是本报告的主要目标。因此,确定了在接受测试期间失效的零件中,包括冲击强度在内的机械性能与试样测试位置深度的关系。另外,以相同的方式研究了具有相同壁厚和不同锻造比的两个测试环。根据ASTM G48进行了耐腐蚀测试,在某些情况下确定了临界点蚀温度(CPT)。通过光学显微镜以及扫描电子显微镜(SEM)和透射电子显微镜(TEM)检查微观结构。使用聚焦离子束(FIB)设备在SEM标本的明显位置对TEM箔进行微加工。

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