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Synthesis and Characterization of SiO_2Coating - on Cast Pure Titanium

机译:铸造纯钛表面SiO_2涂层的合成与表征。

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The silicon coating was deposited by sol–gel dipping process as intermediate layer to minimize titanium oxidation for Ti-porcelain restorat ons. The effect of silicon coating on bonding strength of titanium–porcelain was investigated. The adhesion between the titanium and porcelain was evaluated by three-point flexure bonding test. The result of TG-DSC analysis showed that the optimal treating temperature for SiO_2 coating was 300℃. Silicon coating was effective in preventing titanium oxide layer formation and improving bonding strength. The improvement in bonding strength of titanium–porcelain was about 10%. At the same time, the in vitro bioactivity of the titanium and SiO_2 coating was studied by cytotoxicity test. The methyl thiazolyl tetrazolium assay results demonstrated that the cytotoxicities of SiO_2 coating were ranked as 0. The SEM results revealed the existence of microcrack on the SiO_2 coating surface. Failure of the titanium–porcelain predominantly occurred at the titanium-oxide interface. The SiO_2 coating increased bonding strength of titanium–porcelain and could be used for dental implant materials.
机译:硅涂层通过溶胶-凝胶浸渍工艺沉积为中间层,以最大程度地减少钛瓷修复体中的钛氧化。研究了硅涂层对钛瓷结合强度的影响。钛和瓷之间的粘合性通过三点弯曲粘合试验评价。 TG-DSC分析结果表明,SiO_2涂层的最佳处理温度为300℃。硅涂层有效地防止了氧化钛层的形成并提高了粘结强度。钛瓷的粘结强度提高了约10%。同时,通过细胞毒性试验研究了钛和SiO_2涂层的体外生物活性。甲基噻唑基四唑鎓测定结果表明,SiO_2涂层的细胞毒性为0。SEM结果表明,SiO_2涂层表面存在微裂纹。钛瓷的失效主要发生在钛氧化物界面。 SiO_2涂层提高了钛瓷的粘合强度,可用于牙种植体材料。

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