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Encapsulation of cinnamon essential oil in electrospun nanofibrous film for active food packaging

机译:肉桂精油在电纺纳米纤维薄膜中的封装,用于活性食品包装

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摘要

Electrospun polyvinyl alcohol/cinnamon essential oilffi-cyclodextrin (PVA/CEO/P-CD) antimicrobial nanofibrous film with average diameter 240 +/- 40 nm was successfully fabricated under the optimal conditions. The data of attenuated total reflectance-Fourier transform infrared spectroscopy (ATR-FTIR) and thermogravimetric analysis (TGA) indicated that CEO was encapsulated into beta-CD cavity and there existed molecular interaction among PVA, CEO and beta-CD, which enhanced the thermal stability of CEO. Water contact angle analysis showed that addition of CEO/beta-CD made the nanofibrous film more hydrophilic. The PVA/CEO/beta-CD nanofibrous film exhibited excellent antimicrobial activity, and its minimum inhibitory concentration (MIC) against Staphylococcus aureus and Escherichia coli was approximate 0.9-1 mg/mL (corresponding CEO concentration 8.9-9.9 mu g/mL) and minimum bactericidal concentration (MBC) was approximate 7-8 mg/mL (corresponding CEO concentration 693-79.2 mu g/mL). Furthermore, the mild electrospinning process was favorable for maintaining greater CEO in the film resulting in an improved antimicrobial activity compared with that of casting film. In addition, the PVA/CEO/beta-CD nanofibrous film can effectively prolong the shelf-life of strawberry, indicating it is potential for the application in active food packaging. (C) 2015 Elsevier Ltd. All rights reserved.
机译:在最佳条件下成功制备了电纺聚乙烯醇/肉桂精油氟环糊精(PVA / CEO / P-CD)抗菌纳米纤维膜,其平均直径为240 +/- 40 nm。衰减全反射-傅立叶变换红外光谱(ATR-FTIR)和热重分析(TGA)的数据表明,CEO被封装在β-CD腔中,PVA,CEO和β-CD之间存在分子相互作用,从而增强了热首席执行官的稳定性。水接触角分析表明,CEO /β-CD的加入使纳米纤维膜更加亲水。 PVA / CEO /β-CD纳米纤维膜表现出优异的抗菌活性,其对金黄色葡萄球菌和大肠杆菌的最低抑菌浓度(MIC)约为0.9-1 mg / mL(相应的CEO浓度为8.9-9.9μg / mL),最低杀菌浓度(MBC)约为7-8 mg / mL(相应的CEO浓度为693-79.2μg / mL)。此外,与流延膜相比,温和的静电纺丝工艺有利于在膜中保持更大的CEO,从而提高了抗菌活性。此外,PVA / CEO /β-CD纳米纤维膜可有效延长草莓的保质期,表明其在活性食品包装中的应用潜力。 (C)2015 Elsevier Ltd.保留所有权利。

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