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Synthesis and Characterization of Iron Oxide Nanoparticles Using Amphiphilic Diblock Copolymer PS-b-PAA Micelle as Soft Template

机译:以两亲性二嵌段共聚物PS-b-PAA胶束为软模板的氧化铁纳米粒子的合成与表征

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摘要

By hydrothermal treatment, α-Fe2O3 with club and date pit-like structures were successfully prepared using amphiphilic diblock copolymer poly(styrene-b-acrylic acid) (PS-b-PAA) micelle as soft template. The particles were characterized by fourier transform infrared (FTIR), powder X-ray diffraction (XRD), scanning electron microscopy (SEM). The influence of factors on the morphologies of α-Fe2O3 particles, such as the compositions and concentration of copolymer, and existence of citric acid, has been discussed.
机译:通过水热处理,以两亲性二嵌段共聚物聚苯乙烯-b-丙烯酸(PS-b-PAA)胶束为软模板,成功制备了具有棍状和枣核状结构的α-Fe2O3。通过傅里叶变换红外(FTIR),粉末X射线衍射(XRD),扫描电子显微镜(SEM)对颗粒进行表征。讨论了影响α-Fe2O3颗粒形态的因素,例如共聚物的组成和浓度以及柠檬酸的存在。

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