Isolation and Structural Characterization of the Most Stable, Highly Symmetric Isomer of C_(60)(CF_3)_(18)

Nadezhda A. Samokhvalova; Pavel A. Khavrel; Vitally Yu. Markov; Pavel S. Samokhvalov; Alexey A. Goruynkov; Erhard Kemnitz; Lev N. Sidorov; Sergey I. Troyanov

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Isolation and Structural Characterization of the Most Stable, Highly Symmetric Isomer of C_(60)(CF_3)_(18)

机译：C_（60）（CF_3）_（18）最稳定，高度对称的异构体的分离和结构表征

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摘要

The high thermal and chemical stability of C_(3v)-C_(60)(CF_3)_(18) al_lowed its isolation from a complex C_(60)(CF_3)_n isomer mixture followed by characterization with ~(19)F NMR spectroscopy and single-crystal X-ray crystallography.

机译：C_（3v）-C_（60）（CF_3）_（18）的高热稳定性和化学稳定性使其可以从复杂的C_（60）（CF_3）_n异构体混合物中分离出来，然后用〜（19）F NMR光谱进行表征和单晶X射线晶体学。

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《European journal of organic chemistry》 |2009年第18期|共4页
作者
Nadezhda A. Samokhvalova; Pavel A. Khavrel; Vitally Yu. Markov; Pavel S. Samokhvalov; Alexey A. Goruynkov; Erhard Kemnitz; Lev N. Sidorov; Sergey I. Troyanov;
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原文格式 PDF
正文语种 eng
中图分类 540E0002;
关键词
Fullerenes; Trifluoromethylation; NMR spectroscopy; Structure elucidation;

机译：富勒烯;三氟甲基化;NMR光谱;结构解析;

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1. Isolation and Structural Characterization of the Most Stable, Highly Symmetric Isomer of C_(60)(CF_3)_(18) [J] . Nadezhda A. Samokhvalova, Pavel A. Khavrel, Vitally Yu. Markov, European journal of organic chemistry . 2009,第18期

机译：C_（60）（CF_3）_（18）最稳定，高度对称的异构体的分离和结构表征
2. Synthesis, isolation, and addition patterns of trifluoromethylated D _(5h) and I_h isomers of Sc_3N@C_(80): Sc_3N@D_(5h)-C_(80)(CF_3)_(18) and Sc_3N@Ih-C_(80)(CF_3)_(14) [J] . Yang S., Chen C., Jiao M., Inorganic Chemistry: A Research Journal that Includes Bioinorganic, Catalytic, Organometallic, Solid-State, and Synthetic Chemistry and Reaction Dynamics . 2011,第8期

机译：Sc_3N @ C_（80）的三氟甲基化D _（5h）和I_h异构体的合成，分离和加成模式：Sc_3N @ D_（5h）-C_（80）（CF_3）_（18）和Sc_3N @ Ih-C_（ 80）（CF_3）_（14）
3. Isolation and structural characterization of the most highly trifIuoromethylated C_(70) fullerenes: C_(70)(CF3)_(18) and C_(70)(CF3)_(20) [J] . D. V. Ignateva, A. A. Goryunkov, N. B. Tamm New Journal of Chemistry . 2013,第2期

机译：高度三氟甲基化的C_（70）富勒烯的分离和结构表征：C_（70）（CF3）_（18）和C_（70）（CF3）_（20）
4. VIBRATIONAL SPECTRA AND MOLECULAR STRUCTURE OF THE HYDROFULLERENES C_(60)H_(18), C_(60)D_(18), AND C_(60)H_(36) AS STUDIED BY IR AND RAMAN SPECTROSCOPY AND FIRST-PRINCIPLE CALCULATIONS [C] . A.A. POPOV, V.V. SENYAVIN, A.A. GRANOVSKY, NATO Advanced Research Workshop on Hydrogen Materials Science and Chemistry of Carbon Nanomaterials; 20030914-20; Sudak, Crimea(UA) . 2003

机译：红外和拉曼光谱及第一性原理研究的富勒烯C_（60）H_（18），C_（60）D_（18）和C_（60）H_（36）的振动光谱和分子结构
5. Complexes of large metal ions with symmetrically substituted 6-N-donor macrocyclic ligands: Synthesis, structural studies, and characterization of isomers. [D] . Smetana, Kristine Samaria. 2004

机译：具有对称取代的6-N供体大环配体的大金属离子的配合物：异构体的合成，结构研究和表征。
6. Isolation and characterization of a 60-residue intestinal peptide structurally related to the pancreatic secretory type of trypsin inhibitor: influence on insulin secretion. [O] . B Agerberth, J Söderling-Barros, H Jörnvall, 1989

机译：与胰蛋白酶抑制剂的胰腺分泌型结构相关的60个残基肠肽的分离和表征：对胰岛素分泌的影响。
7. First-principles calculations of the structural, electronic, vibrational and magnetic properties of C_{60} and C_{48}N_{12}: a comparative study [O] . Xie, Rui-Hua, Bryant, Garnett W., Jensen, Lasse, 2003

机译：结构，电子，振动的第一性原理计算和C_ {60}和C_ {48} N_ {12}的磁性：比较研究
8. Isolation of a Stable Binuclear Copper Complex Containing a Copper-Copper Bonded Unit. The X-Ray Structure Determination ((7,8,15,16,17,18,25,26,33,34,35,36- Dodecahydrotetrabenzo(e,m,s,a')(1,4,8,11,15,18,22,25)Octa-Azacyclo- Octa [R] . Dancey, K. P., Tasker, P. A., Price, R., 1980

机译：含有铜 - 铜键合单元的稳定双核铜配合物的分离。 X射线结构测定（（7,8,15,16,17,18,25,26,33,34,35,36-Dodecahydrotetrabenzo（e，m，s，a'）（1,4,8， 11,15,18,22,25）Octa-azacyclo- Octa

Isolation and Structural Characterization of the Most Stable, Highly Symmetric Isomer of C_(60)(CF_3)_(18)

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