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Fabrication of Silver Nanoparticles Decorated on Activated Screen Printed Carbon Electrode and Its Application for Ultrasensitive Detection of Dopamine

机译:活性丝网印刷碳电极修饰的纳米银的制备及其在多巴胺超灵敏检测中的应用

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摘要

In the present study, we report the fabrication of silver nanoparticles (AgNPs) decorated on activated screen printed carbon electrode (ASPCE). The AgNPs were prepared by using Justicia glauca leaf extract as a reducing and stabilizing agent and the ASPCE was prepared by a simple electrochemical activation of screen printed carbon electrode (SPCE). The ASPCE/AgNPs shows a reversible electrochemical behaviour with enhanced response for DA than that of other modified SPCEs. Under optimum conditions, the electrochemical oxidation current response of DA is linear over the concentration range from 0.05 to 45.35 mu M. The limit of detection is found as 0.017 mu M with a high sensitivity of 7.85 mu A mu M-1 cm(-2).
机译:在本研究中,我们报告了在活性丝网印刷碳电极(ASPCE)上装饰的银纳米颗粒(AgNP)的制造。通过使用Justicia glauca叶提取物作为还原剂和稳定剂来制备AgNP,并通过简单的丝网印刷碳电极(SPCE)的电化学活化来制备ASPCE。与其他修饰的SPCE相比,ASPCE / AgNPs具有可逆的电化学行为,对DA的响应增强。在最佳条件下,DA的电化学氧化电流响应在0.05至45.35μM的浓度范围内呈线性。检测限为0.017μM,高灵敏度为7.85μAμM-1 cm(-2) )。

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