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A Pulse Nuclear Quadrupole Resonance Spectrometer

机译:脉冲核四极共振光谱仪

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摘要

A pulse nuclear quadrupole resonance (NQR) spectrometer intended for studying the resonance signal spectra of nuclei of solid substances in a 1- to 30-MHz band is described. The pulse duration of excitation pulses is regulated from 10 to 100 μs at a 5- to 100-Hz pulse repetition rate. The spectrometer ensures a probing pulse power of up to 1.5 kW and is characterized by the availability of an NQR signal simulator, a low-noise preamplifier, and a phase detector with a dynamic range exceeding 100 dB. The efficiency of the spectrometer has been tested by studying the NQR spectrum of ~(14)N nuclei in urotropine. The spectrometer ensured a possibility of detecting 0.2 g of urotropine.
机译:描述了一种脉冲核四极共振(NQR)光谱仪,该光谱仪旨在研究1到30 MHz频带中固体物质核的共振信号光谱。激励脉冲的脉冲持续时间以5到100 Hz的脉冲重复频率从10到100μs调节。该光谱仪可确保高达1.5 kW的探测脉冲功率,其特点是具有NQR信号模拟器,低噪声前置放大器和动态范围超过100 dB的鉴相器。光谱仪的效率已通过研究乌托品中〜(14)N核的NQR光谱进行了测试。光谱仪确保了检出0.2 g乌罗托品的可能性。

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