The reaction of alpha-halocarbonyl compounds with (NH4)OH, (NH4)(2)SO4 or NH4Cl solution under microwave-irradiation

Utsukihara Takamitsu; Koshimura Masahiro; Kitsuta Kazunori; Sato Akinori; Matsushita Masatoshi; Takahashi T. Tomoyoshi; Horiuchi C. Akira

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The reaction of alpha-halocarbonyl compounds with (NH4)OH, (NH4)(2)SO4 or NH4Cl solution under microwave-irradiation

机译：微波辐射下α-卤代羰基化合物与（NH4）OH，（NH4）（2）SO4或NH4Cl溶液的反应

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摘要

Reaction of alpha-halo ketone (alpha-bromo ketone) under microwave irradiation gives the pyrazine and quinoxaline derivative in good yields. This reaction affords a clean and convenient synthetic method for pyrazine and quinoxaline derivatives.

机译：微波辐射下α-卤代酮（α-溴代酮）的反应以良好的收率得到了吡嗪和喹喔啉衍生物。该反应提供了吡嗪和喹喔啉衍生物的清洁和方便的合成方法。

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《Indian Journal of Chemistry, Section B. Organic Including Medicinal》 |2016年第12期|共8页
作者
Utsukihara Takamitsu; Koshimura Masahiro; Kitsuta Kazunori; Sato Akinori; Matsushita Masatoshi; Takahashi T. Tomoyoshi; Horiuchi C. Akira;
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正文语种 eng
中图分类化学;
关键词
alpha-halo ketone; pyrazine; quinoxaline; 1; 2-phenylenediamine; microwave;

机译：α-卤代酮;吡嗪;喹喔啉;1;2-苯二胺;微波;

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1. 硅酸盐在（NH4）2WO4-（NH4）2CO3-NH3-H2O体系中反应行为的热力学分析 [J] . 李小斌, 申雷霆, 童潇依, 中国有色金属学报：英文版 . 2018,第011期
2. The reaction of alpha-halocarbonyl compounds with (NH4)OH, (NH4)(2)SO4 or NH4Cl solution under microwave-irradiation [J] . Utsukihara Takamitsu, Koshimura Masahiro, Kitsuta Kazunori, Indian Journal of Chemistry, Section B. Organic Including Medicinal . 2016,第12期

机译：微波辐射下α-卤代羰基化合物与（NH4）OH，（NH4）（2）SO4或NH4Cl溶液的反应
3. MgF2 Solubility in MgF2 + Salt + H2O Systems (Salt = MgSO4, (NH4)(2)SO4, NH4Cl) at 298.15 K [J] . Li Hongliang, Xu Chao, Tan Ze, Journal of Chemical and Engineering Data: the ACS Journal for Data . 2019,第1期

机译：MgF2溶液中的MgF2 + H2O系统（盐= MgSO4，（NH4）（2）SO4，NH 4 Cl），298.15 k
4. The inhibition effect of SeO2 on hydrogen evolution reaction in MnSO4-(NH4)(2)SO4 solution [J] . Jiao Pengpeng, Xu Fuyuan, Li Jianhui, International journal of hydrogen energy . 2016,第2期

机译：SeO2对MnSO4-（NH4）（2）SO4溶液中析氢反应的抑制作用
5. MECHANICAL AND INTERFACIAL PROPERTIES OF CARBON FIBER MODIFIED BY ELECTROCHEMICAL OXIDATION IN (NH4HCO3)/(NH4)2C2O4·H2O AQUEOUS COMPOUND SOLUTION [C] . Yuli Tian, Jie Liu, Jieying Liang Annual World Conference on Carbon . 2010

机译：（NH4HCO3）/（NH4）/（NH4）2C204·H2O水合物溶液中电化学氧化改性碳纤维的机械和界面性能
6. The study of liquid solution and solid phase systems: I. Reactions and thermodynamics of alkyl halides. II. Structures and energetics of group 13-15 compounds. [D] . Kormos, Bethany Lyn. 2004

机译：液相和固相系统的研究：I.卤代烷的反应和热力学。二。 13-15组化合物的结构和能量。
7. Ammonium iron(III) phosphate(V) fluoride (NH4)0.5(NH4)0.375K0.125FePO4F with ammonium partially substituted by potassium [O] . Lei Wang, Yan Zhou, Ya-Xi Huang, 2009

机译：磷酸铁（III）（V）氟化铵（NH4）0.5 （NH4）0.375K0.125 FePO4F铵的一部分被钾取代
8. Uranyl(VI) Compounds. I. The Crystal Structure of Ammonium Uranyl Sulfate Dihydrate, (NH4)2UO2(SO4)2.2H2O. [O] . Lauri Niinistö, Jukka Toivonen, Jussi Valkonen, 1978

机译：铀酰（VI）化合物。 I.硫酸铵二水合物的晶体结构，（NH4）200O2（SO 4）2.2H2O。
9. A Mossbauer Effect Study of Electronic Relaxation in the Paramagnetic Compound: NH4(Fe,A1l)(SO4)2 . 12 H2o [R] . Campbell, L. E. 1966

机译：顺磁性化合物电子弛豫的穆斯堡尔效应研究：NH4（Fe，all）（sO4）2。 12 H2o

The reaction of alpha-halocarbonyl compounds with (NH4)OH, (NH4)(2)SO4 or NH4Cl solution under microwave-irradiation

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