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A STUDY ON THE FABRICATION OF IRON POWDER FROM FORGING SCALE USING HYDROGEN

机译:用氢锻造氧化铁粉制备铁粉的研究

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摘要

This study was conducted to investigate the effect of hydrogen content, temperature, reaction time for the reduction of forging scale which is mainly composed of hematite (Fe2O3). All reductive reactions were performed over the temperature range of 700 to 1200 degrees C as well as 0.1 to 1 atm of hydrogen partial pressures. The results showed that the mechanism for the reduction of iron oxides using hydrogen gas was not a simple process, but proceeded in multiple reduction stages thermodynamically. The iron oxide was almost completely reduced to metallic iron powder with 91 wt.% of iron content in the forging scale at 0.1 atm of hydrogen partial pressure. The content of iron was however found to be increased with increasing hydrogen partial pressure from 0.1 to 1 atm with regardless of temperatures. The metallic iron powder was obtained with the mean size of 100 mu m and more porous structure was observed.
机译:本研究旨在研究氢含量,温度,反应时间对减少主要由赤铁矿(Fe2O3)组成的锻造氧化皮的影响。所有还原反应均在700至1200摄氏度的温度范围以及0.1至1大气压的氢分压下进行。结果表明,用氢气还原氧化铁的机理不是简单的过程,而是在热力学上分多个步骤进行的。在0.1atm的氢分压下,氧化铁几乎完全还原为锻造氧化皮中铁含量为91重量%的金属铁粉。然而发现,无论温度如何,铁含量都随着氢分压从0.1atm增加到1atm而增加。获得平均尺寸为100μm的金属铁粉,并观察到更多的多孔结构。

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