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Thermal shock behavior of multilayer and functionally graded micro- and nano-structured topcoat APS TBCs

机译:多层和功能渐变微型和纳米结构面板APS TBCS的热冲击行为

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摘要

Performance of air plasma sprayed (APS) thermal barrier coatings (TBCs) with multilayer and functionally graded topcoat were investigated in thermal shock conditions. Ceria-yttria stabilized zirconia (CSZ) and micro and nano-structured yttria stabilized zirconia (YSZ and YSZ-N) were used to produce coating samples. The samples were classified into four families, namely single-layer, double-layer, triple-layer and functionally graded (FG). To measure thermal shock resistance, the heating/water quenching cycles were repeated 70 times and 30% destruction of the coating was considered its functionality limit. Thus, cycles did not continue for those coatings that were destroyed more than 30%. At the end of each cycle, the surface and edge damage were determined from the photos of samples. Furthermore, scanning electron microscope (SEM) images and energy-dispersive spectrometer (EDS) analysis of samples' cross-section were taken before and after the test. After collecting the experimental data, effects of various factors on outputs were investigated. The results showed that YSZ-N single-layer coating and triple-layer with CSZ as a top layer, has less thermally grown oxide (TGO) thickness and best performance in thermal shock conditions.
机译:在热冲击条件下研究了具有多层和功能梯度面涂层的空气等离子体喷涂(APS)热阻挡涂层(TBC)。二氧化铈 - 钇稳定的氧化锆(CSZ)和微型和纳米结构yttra稳定的氧化锆(YSZ和YSZ-N)用于生产涂料样品。将样品分为四个家族,即单层,双层,三层和功能分级(FG)。为了测量热抗冲击性,重复加热/水猝灭循环70倍,涂层的破坏30%被认为是其功能限制。因此,循环未持续超过30%的涂层。在每个循环结束时,从样品的照片确定表面和边缘损坏。此外,在试验之前和之后,扫描电子显微镜(SEM)图像和能量分散光谱仪(EDS)分析样本的横截面。收集实验数据后,研究了各种因素对产出的影响。结果表明,YSZ-N单层涂层和用CSZ作为顶层的三层,具有较少的热生长氧化物(TGO)厚度和热冲击条件中的最佳性能。

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