Optimization of Melt-spinning Parameters of Poly(ethylene terephthalate) Partially Oriented Multi-filament Yarn in an Industrial Scale: Central Composite Design Approach

摘要

In this study, central composite design (CCD) based on response surface methodology (RSM) was employed to optimize parameters of melt-spinning process of poly(ethylene terephthalate) partially oriented multifilament yam (POMFY). On the basis of a four-variable CCD, RSM was used to determine the effects of spinning temperature, spinning pressure, take-up velocity and quenching air velocity on the levels of the elongation of POMFY as the response. The POMFY samples were also characterized by scanning electron microscopy (SEM) and energy dispersive X-ray (EDX) analysis. By applying a quadratic regression analysis, an equation indicating the effect of each variables on the response was developed. The predicted values of the parameters showed excellent agreement with the experimental values (R-2=0.9565, Adjusted-R-2=0.916). Moreover, the results confirmed that the CCD mathematical model was a suitable method to optimize the melt spinning parameters of POMFY in an industrial scale.