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首页> 外文期刊>Journal of separation science. >A liquid chromatography with tandem mass spectrometry method to simultaneously determinate chlorpyrifos, imidacloprid and imidacloprid metabolites in wheat
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A liquid chromatography with tandem mass spectrometry method to simultaneously determinate chlorpyrifos, imidacloprid and imidacloprid metabolites in wheat

机译：具有串联质谱法的液相色谱法，同时测定小麦中的紫外线，吡虫啉和咪酰啉代代谢物

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Abstract > A liquid chromatography with tandem mass spectrometry method was developed and validated to simultaneously determine chlorpyrifos, imidacloprid, and imidacloprid metabolites in soil, wheat grain, and wheat straw matrices. Satisfactory linearity (R 2 ≥ 0.9965) of the method was obtained for all analytes. The ranges of limits of detection and limits of quantification for seven analytes in three matrices were 0.17–66.7 and 0.5–200?μg/kg, respectively. Average recoveries were 72.85–81.25% for chlorpyrifos, 78.54–84.70% for imidacloprid, 73.83–81.03% for imidacloprid olefin, 71.47–80.61% for 5‐hydroxy imidacloprid, 71.79–81.32% for imidacloprid urea, 70.42–82.20% for imidacloprid nitroguanidine, and 70.91–82.46% for imidacloprid 6‐chloronicotinic acid in soil, wheat grain, and wheat straw. The intra‐ and interday relative standard deviations were less than 8%. The established method was successfully applied for the residual analysis of chlorpyrifos, imidacloprid, and imidacloprid metabolites in actual soil, wheat grain, and wheat straw samples. The results indicated that the established method could be used to detect trace amounts of chlorpyrifos, imidacloprid, and imidacloprid metabolites in wheat and that the method might be able to provide some data on the detection of these seven compounds in other crops. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“Main”XML：Lang =“En”> <标题类型=“main”>摘要</标题> >具有串联质谱法的液相色谱分析并验证，同时测定毒物吡啶，土壤，小麦籽粒和小麦秸秆基质中的吡虫啉代谢物。对所有分析物获得该方法的令人满意的线性（R <SUP> 2 </ sup>≥0.9965）。三种基质中七种分析物的定量限制的范围分别为0.17-66.7和0.5-200Ωμg/ kg。紫外波吡啶的平均回收率为72.85-81.25％，咪酰啉烯烃的73.83-81.03％73.83-81.03％，5-羟基咪唑啉酮的71.47-80.61％，吡虫啉尿素71.79-81.32％，70.42-82.20％，咪酰啉肼硝基和70.91-82.46％用于土壤，小麦籽粒和小麦秸秆中的吡虫啉6-氯霉素酸。间隔和间隔的相对标准偏差小于8％。成功的方法已成功应用于氯吡啶，吡虫啉和咪酰啉代吡啶的残留分析，实际土壤，小麦籽粒和小麦秸秆样品中的代谢物。结果表明，已建立的方法可用于检测小麦的含踪含量的氯吡啶，吡虫啉和咪酰啉代代谢物，并且该方法可能能够提供一些关于在其他作物中检测这七种化合物的一些数据。 </ p> </ abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-35800/'>《Journal of separation science.》</a> <b style="margin: 0 2px;">|</b><span>2019年第6期</span><b style="margin: 0 2px;">|</b><span>共12页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Huang Min&option=202" target="_blank" rel="nofollow">Huang Min;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Qin Xinxian&option=202" target="_blank" rel="nofollow">Qin Xinxian;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Luo Xiaoshuang&option=202" target="_blank" rel="nofollow">Luo Xiaoshuang;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Yu Weiwei&option=202" target="_blank" rel="nofollow">Yu Weiwei;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Yang Guoqiang&option=202" target="_blank" rel="nofollow">Yang Guoqiang;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Zhang Kankan&option=202" target="_blank" rel="nofollow">Zhang Kankan;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Hu Deyu&option=202" target="_blank" rel="nofollow">Hu Deyu;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>State Key Laboratory Breeding Base of Green Pesticide and Agricultural BioengineeringGuizhou UniversityGuiyang P. R. China;</p> <p>State Key Laboratory Breeding Base of Green Pesticide and Agricultural BioengineeringGuizhou UniversityGuiyang P. R. China;</p> <p>State Key Laboratory Breeding Base of Green Pesticide and Agricultural BioengineeringGuizhou UniversityGuiyang P. R. China;</p> <p>State Key Laboratory Breeding Base of Green Pesticide and Agricultural BioengineeringGuizhou UniversityGuiyang P. R. China;</p> <p>State Key Laboratory Breeding Base of Green Pesticide and Agricultural BioengineeringGuizhou UniversityGuiyang P. R. China;</p> <p>State Key Laboratory Breeding Base of Green Pesticide and Agricultural BioengineeringGuizhou UniversityGuiyang P. R. China;</p> <p>State Key Laboratory Breeding Base of Green Pesticide and Agricultural BioengineeringGuizhou UniversityGuiyang P. R. China;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/159.html" title="化学">化学;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=chlorpyrifos&option=203" rel="nofollow">chlorpyrifos;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=imidacloprid&option=203" rel="nofollow">imidacloprid;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=imidacloprid metabolites&option=203" rel="nofollow">imidacloprid metabolites;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=liquid chromatography&option=203" rel="nofollow">liquid chromatography;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=wheat&option=203" rel="nofollow">wheat;</a> </p> <div class="translation"> 机译：氯吡啶;咪酰啉;咪酰啉代代谢物;液相色谱;小麦; </div> </li> </ul> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/0704025846430.html">A liquid chromatography with tandem mass spectrometry method to simultaneously determinate chlorpyrifos, imidacloprid and imidacloprid metabolites in wheat</a> <b>[J]</b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Huang Min&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Huang Min,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Qin Xinxian&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Qin Xinxian,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Luo Xiaoshuang&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Luo Xiaoshuang,</a> <a href="/journal-foreign-35800/" target="_blank" rel="nofollow" class="tuijian_authcolor">Journal of separation science. .</a> <span>2019</span><span>,第6期</span> </span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：具有串联质谱法的液相色谱法，同时测定小麦中的紫外线，吡虫啉和咪酰啉代代谢物</span> </p> </li> <li> <div> <b>2. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/0704025935630.html">Determination of imidacloprid and its relevant metabolites in tomato using modified QuEChERS combined with ultrahigh‐pressure liquid chromatography/Orbitrap tandem mass spectrometry</a> <b>[J]</b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Li Junfang&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Li Junfang,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Jiang Yuwei&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Jiang Yuwei,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Li Deqiang&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Li Deqiang </a> <a href="/journal-foreign-36152/" target="_blank" rel="nofollow" class="tuijian_authcolor">Journal of the Science of Food and Agriculture .</a> <span>2019</span><span>,第11期</span> </span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：用改性QueCher结合超高压液相色谱/绕组串联质谱法测定番茄中咪酰啉及其相关代谢物及其相关代谢物</span> </p> </li> <li> <div> <b>3. </b><a class="enjiyixqcontent" href="/academic-journal-foreign_food-chemistry_thesis/020413214445.html">Determination of acetamiprid, imidacloprid, and spirotetramat and their relevant metabolites in pistachio using modified QuEChERS combined with liquid chromatography-tandem mass spectrometry</a> <b>[J]</b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Faraji Mohammad&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Faraji Mohammad,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Noorbakhsh Roya&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Noorbakhsh Roya,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Shafieyan Hooshang&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Shafieyan Hooshang,</a> <a href="/journal-foreign-2358/" target="_blank" rel="nofollow" class="tuijian_authcolor">Food Chemistry .</a> <span>2018</span><span>,第feba1期</span> </span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：改进的QuEChERS结合液相色谱-串联质谱法测定开心果中的乙酰胺，吡虫啉和螺旋体及其相关代谢物</span> </p> </li> <li> <div> <b>4. </b><a class="enjiyixqcontent" href="/academic-conference-foreign_meeting-257539_thesis/0705010726304.html">Determination of chlorpyrifos and its metabolites in cell media using liquid chromatography/electrospray ionization tandem mass spectrometry</a> <b>[C]</b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Feng Liang&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Feng Liang,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Alvin V. 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