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Effect of light-curing units on the thermal expansion of resin nanocomposites.

机译:光固化单元对树脂纳米复合材料热膨胀的影响。

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PURPOSE: To examine the thermal expansion of resin nanocomposites after light-curing using different light-curing units. METHODS: Four different resin nanocomposites and four different light-curing units [quartz-tungsten-halogen (QTH), light emitting diode (LED), laser, and plasma arc] were chosen. Metal dies were filled with resin to make specimens and light-cured. The light intensity and light-curing time of the QTH and LED light-curing units were 1000 mW/cm2 and 40 seconds, 700 mW/cm2 and 40 seconds for the laser, and 1600 mW/cm2 and 3 seconds for the plasma arc. The coefficient of thermal expansion (CTE) was evaluated using a thermomechanical analyzer (TMA) at temperatures ranging from 30-80 degrees C. RESULTS: The CTE of the resin nanocomposites tested ranged from 28.5 to 65.8 (x 10(-6)/ degrees C), depending on the product and type of light-curing unit used. Among the specimens, Grandio showed the lowest CTE. The specimens cured using the plasma arc unit (Apollo 95E) showed the highest CTE. There was a linear correlation between the CTE and filler content (vol%) (R: -0.94-0.99 depending on the light-curing unit). The results may suggest a careful selection of the light-curing unit because there was more expansion in the specimens cured using the plasma arc unit than those cured by the other units.
机译:目的:研究使用不同的光固化单元在光固化后树脂纳米复合材料的热膨胀。方法:选择四种不同的树脂纳米复合材料和四种不同的光固化单元[石英-钨-卤素(QTH),发光二极管(LED),激光和等离子弧]。在金属模具中填充树脂以制成样品并进行光固化。 QTH和LED光固化单元的光强度和光固化时间分别为1000 mW / cm2和40秒,激光700 mW / cm2和40秒,等离子弧为1600 mW / cm2和3秒。使用热机械分析仪(TMA)在30-80摄氏度的温度范围内评估热膨胀系数(CTE)。结果:测试的树脂纳米复合材料的CTE范围为28.5至65.8(x 10(-6)/度) C),取决于产品和所用光固化单元的类型。在样本中,Grandio的CTE最低。使用等离子弧单元(Apollo 95E)固化的样品显示出最高的CTE。 CTE和填料含量(体积%)之间存在线性关系(R:-0.94-0.99,取决于光固化单元)。结果可能表明应谨慎选择光固化单元,因为使用等离子弧单元固化的样品比通过其他单元固化的样品具有更大的膨胀。

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