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Determination of Young's modulus of ceramics from flexural vibration at elevated temperatures

机译:高温弯曲振动法测定陶瓷的杨氏模量

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摘要

In this paper we describe the construction of a laboratory-made resonant apparatus for the modulated force thermomechanical analysis (mf-TMA) and estimate the uncertainty of the measurement of Young's modulus of a porcelain sample. The porcelain sample was measured while increasing the temperature up to 1000 ?C/5 ?C/min. Thermodilatometry was performed to determine the actual dimensions of the sample in the same temperature regime. We assessed the influence of the repeatability of the directly measured values, the accuracy of the used measurers and different exceptions from the ideal experimental arrangement on the Young's modulus measurement uncertainties of types A and B. We found that the majority of the total uncertainty (80%) is determined at the room temperature. The remaining sources of uncertainty can be attributed to thermal expansion of the sample and inhomogeneity of the temperature field. The relative expanded uncertainty of the Young's modulus at the elevated temperatures was 1.1%.
机译:在本文中,我们描述了用于调制力热机械分析(mf-TMA)的实验室制造的谐振装置的构造,并估计了瓷器样品的杨氏模量的不确定性。在将温度升至1000°C / 5°C / min的同时测量瓷器样品。进行热膨胀测定法以确定在相同温度范围内样品的实际尺寸。我们评估了直接测量值的可重复性,使用的测量仪的精度以及理想实验安排中的不同例外情况对A和B型杨氏模量测量不确定度的影响。我们发现,总不确定度的大部分(80 %)是在室温下测定的。不确定性的其余来源可归因于样品的热膨胀和温度场的不均匀性。高温下杨氏模量的相对扩展不确定度为1.1%。

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