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Glutamic acid‐related hydrazine reagent for the derivatization of carbonyl compounds

机译：谷氨酸相关的肼试剂用于羰基化合物的衍生化

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Abstract >Chemical derivatization of carbonyl compounds is a prerequisite for their determination in environmental and biological samples by liquid chromatography‐tandem mass spectrometry analysis. The main requirements regarding the good derivatization reagent are fast, selective, and quantitative reaction with carbonyl compounds and efficient fragmentation upon collision‐induced dissociation. We have prepared glutamic acid‐related hydrazine reagent and optimized derivatization procedure with benzaldehyde as a model carbonyl compound. The collision‐induced dissociation spectrum of the obtained hydrazone gave rich fragmentation pattern with numerous abundant fragment ions. Structure‐specific fragment ions were selected for the development of sensitive multiple reaction monitoring method. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract XMLNS =“http://www.wiley.com/namespaces/wiley”type =“main”xml：lang =“hr”> <title type =“main”>抽象</ title> >化学衍生化羰基化合物是通过液相色谱 - 串联质谱分析在环境和生物样品中测定的先决条件。关于良好衍生化试剂的主要要求是与羰基化合物的快速，选择性和定量反应，并在碰撞诱导的解离时有效的碎片。我们制备了与苯甲醛的谷氨酸相关的肼试剂和优化的衍生化程序作为模型羰基化合物。所得腙的碰撞诱导的解离光谱具有丰富的碎片图案，具有许多丰富的片段离子。选择特异性碎片离子用于开发敏感的多反应监测方法。</ p> </摘要> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-34906/'>《Journal of mass spectrometry: JMS》</a> <b style="margin: 0 2px;">|</b><span>2018年第8期</span><b style="margin: 0 2px;">|</b><span>共6页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Brklja?i? Lidija&option=202" target="_blank" rel="nofollow">Brklja?i? Lidija;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Jeri? Ivanka&option=202" target="_blank" rel="nofollow">Jeri? Ivanka;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Division of Organic Chemistry and BiochemistryRu?er Bo?kovi? InstituteBijeni?ka cesta 54 10000 Zagreb Croatia;</p> <p>Division of Organic Chemistry and BiochemistryRu?er Bo?kovi? InstituteBijeni?ka cesta 54 10000 Zagreb Croatia;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/1187.html" title="分析化学">分析化学;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=carbonyl compounds&option=203" rel="nofollow">carbonyl compounds;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=derivatization&option=203" rel="nofollow">derivatization;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=hydrazine reagent&option=203" rel="nofollow">hydrazine reagent;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=hydrazones&option=203" rel="nofollow">hydrazones;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=MS/MS analysis&option=203" rel="nofollow">MS/MS analysis;</a> </p> <div class="translation"> 机译：羰基化合物;衍生化;肼试剂;腙;MS / MS分析; </div> </li> </ul> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/0704025632990.html">Glutamic acid‐related hydrazine reagent for the derivatization of carbonyl compounds</a> <b>[J]</b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Brklja?i? 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