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Sensitive 1,2-dichlorobenzene chemi-sensor development based on solvothermally prepared FeO/CdO nanocubes for environmental safety

机译:基于溶剂热制备的FeO / CDO纳米尺寸的环境安全敏感1,2-二氯苯化学传感器开发

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摘要

In this approach, we report the assembly of a dynamic, high sensitive, selective and reproducible 1,2-dichlorobenzene (1,2-DCB) chemi-sensor development based on solvothermally prepared nanocubes (NCs) of FeO/CdO. The synthesized FeO/CdO NCs was exhibited as an excellent electron mediator during the sensing performance of 1,2-DCB in aqueous medium and this research work was executed by electrochemical method. The morphological, optical, elemental, and structural characterization of synthesized NCs were investigated by various conventional techniques such as FTIR, UV-vis, FESEM, XPS, EDS, and XRD. NCs were used to fabricate glassy carbon electrode (GCE) with nation conducting binder. The sensitivity of proposed chemi-sensor was estimated from the slope of calibration curve attained as current versus concentration of 1,2-DCB relation. It was introduced a reliable future sensitive sensor development using FeO/CdO NCs by electrochemical approach for the probable detection of toxic 1,2-DCB and other environmental carcinogenic chemicals for the safety of environmental and health care fields. (C) 2018 The Korean Society of Industrial and Engineering Chemistry. Published by Elsevier B.V. All rights reserved.
机译:在这种方法中,我们报告了基于FeO / CDO的溶剂热制备的纳米尺(NCS)的动态,高敏感,选择性和可重复的1,2-二氯苯(1,2-DCB)化学传感器开发的组装。在含水介质中1,2-DCB的感测性能期间,作为优异的电子介体在1,2-DCB的感测性能下,通过电化学方法执行合成的FOO / CDO NC。通过各种常规技术(如FTIR,UV-Vis,FESEM,XPS,EDS和XRD)研究了合成NCS的形态学,光学,元素和结构表征。 NCS用于用Nation导电粘合剂制造玻璃碳电极(GCE)。从校准曲线的斜率估计所提出的化学传感器的灵敏度,作为电流与1,2-DCB关系的浓度。通过电化学方法引入了可靠的未来敏感传感器开发,用于通过电化学方法进行有可能检测毒性1,2-DCB和其他环境致癌物质的安全性保护区。 (c)2018年韩国工程和工程化学学会。 elsevier b.v出版。保留所有权利。

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